Instruction Manual
INFRARED GAS
ANALYZER
TYPE: ZSP
INZ-TN4ZSPb-E
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CAUTION ON SAFETY
Before use, carefully read this “Caution on safety” so that the product is usable correctly.
• The precautions given here are of great significance to safety. Therefore, they should be observed without fail.
The precautions on safety are classified into ranks “Danger”, “Caution” and “Prohibition.”
Danger
Items which pertains to incorrect handling that may lead to personal death
or serious injury
Caution
Items which pertains to incorrect handling that may lead to medium trouble,
injury or physical damage
Prohibition
Items which pertains to prohibition (DO NOT)
Installation, carrying, relocation and storage of gas analyzer
Danger
• This product is not explosion-proof. Do not use it in explosive gas-rich atmosphere. Otherwise,
serious accidents such as explosion and fire may be caused.
Caution
• Installation, carrying and relocation must be made by a qualified contractor or your dealer.
Incorrect installation results in falling accidents, electric shocks or fire accidents.
• The gas analyzer is heavy. Special care should be taken for installation to prevent trouble or injury due
to falling or dropping of the analyzer.
• When the gas analyzer needs to be lifted, be sure to put on gloves. Do not hold it with bare hands to
prevent injury.
• This product must be installed in a place that meets the conditions specified in the ‘instruction manual’
Use in a place that is outside the given installation conditions may cause an electric shock, fire or
malfunction.
• During installation work, attention should be paid not to allow entrance of wire fragments, etc. into the
product. Otherwise, a fire, trouble or malfunction may be caused.
– ii –
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Caution on wiring
Caution
• Request an installation company or your dealer to carry out wiring.
If wiring is incomplete, shock hazard or injury may be caused.
• Class D grounding construction is mandatory. Otherwise, shock hazard may be caused.
< Caution for wiring company >
For preventing shock hazard, fire and injury, be sure to observe the following.
• Before wiring, be sure to turn off the primary power supply. If this is neglected, you may receive an
electric shock.
• For grounding, use a 600 V-IV wire having a diameter of 2 mm2 or more and an adequate dielectric
strength.
• Connect the power supply which meets the rating of product. Connection of other power supply may
cause a fire.
• Select the diameter of input and output wires, which matches the rated current of gas analyzer.
• Be sure to use solderless terminals for connection to the input and output terminal block.
• Use the terminal block for branching the output wire.
• Be sure to fix the input and output wires onto the floor, wall surface, etc. and use a protective device
for wires.
Caution on use
Danger
• If you notice malodor or abnormal sound, stop the instrument immediately. If this is neglected, fire
may occur.
Caution
• When the analyzer is to be operated after it has been left unused for a long time, the operating proce-
dure is different from the normal stop/start procedure. It should be handled according to the procedure
shown in the instruction manual to ensure its proper performance and to prevent trouble or injury.
• Do not operate the analyzer for a long time with its door left open to avoid entry of dust into the
analyzer. Dust deposits will result in damage to the analyzer.
– iii –
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Caution on use
Prohibition
• Do not insert a rod or your finger into the fan (electronic cooler at ceiling), otherwise injury may be
caused by the rotating blades.
• Do not touch metal, finger, etc. to the input and output terminal block of analyzer. Otherwise, shock
hazard or injury may be caused.
• Smoking and use of fire/flame is prohibited in the vicinity of the gas analyzer. Otherwise, a fire may
occur.
• A water-filled container such as a bucket should not be placed on the roof of the gas analyzer having
indoor specifications. If such a container turns over, spilled water may cause shock hazard or burning
inside the analyzer.
Caution on maintenance / inspection
Danger
• When handling standard gas such as calibration gas, read the instruction manual for the standard gas
for correct handling. Special care should be taken when handling hazardous gas such as CO gas and
the like to prevent poisoning.
• During maintenance or inspection, be sure to turn ON the ventilation fan in the analyzer to prevent
poisoning due to gas leakage.
• When the gas filter of the analyzer is to be replaced or the washing unit needs maintenance, be sure to
close the calibration gas valve. Especially, if the calibration gas valve is located at the sample gas
inlet, the replacing or washing shall be done after closing the calibration gas valve to prevent poison-
ing or other trouble.
Caution
• The gas converter is heated to about 220°C. When the catalytic agent needs to be replaced, turn OFF
the power for the converter and use heat-proof gloves about 30 minutes later.
• When the fuse is blown off, check the cause of it and replace it with the same type of fuse having the
same capacity to prevent electric shocks or other trouble.
• When the analyzer is provided with a power leak relay, press the test button to confirm proper opera-
tion before making maintenance or inspection to prevent electric shocks.
• Be sure to lock the door. Do not allow unauthorized persons to use the door key. Do not touch the
door carelessly to prevent electric shocks and other trouble.
The following items must be observed to prevent electric shocks or injury and to ensure safety.
• Take off metallic objects such as wrist watch before starting the work.
• Do not touch the device with wet hands.
– iv –
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Others
Caution
• When trouble cannot be remedied even after following the instruction manual, contact your dealer or
Fuji's service station (serivice engineer). Do not disassemble the device, as it results in electric shocks
or injury.
• Do not use replacement parts which are not specified by makers. Use of these parts will not only
provide the required performance but also result in damage or other trouble.
• Replacement parts used for maintenance must be handled as incombustible objects.
– v –
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CONTENTS
INTRODUCTION ................................................................................................................................................... i
CAUTION ON SAFETY ....................................................................................................................................... ii
1. OUTLINE ....................................................................................................................................................... 1
2. SPECIFICATIONS ........................................................................................................................................ 1
3. COMPOSITION ............................................................................................................................................. 1
4. INSTALLATION ........................................................................................................................................... 2
4.1
4.2
4.3
4.4
4.5
Selection of installation site ................................................................................................................ 2
Selection of gas sampling location ...................................................................................................... 2
Installation work.................................................................................................................................. 3
Connection of cables ........................................................................................................................... 3
Connection of pipes............................................................................................................................. 3
5. DESCRIPTION OF EACH PART ................................................................................................................. 5
6. PREPARATION FOR OPERATION ............................................................................................................ 5
6.1
6.2
6.3
6.4
6.5
6.6
Injection of clean water ....................................................................................................................... 5
Supply of external power .................................................................................................................... 5
Check of sample piping, exhaust piping, etc....................................................................................... 5
Airtightness test ................................................................................................................................... 6
Setting of temperature inside locker.................................................................................................... 6
Warm-up time ..................................................................................................................................... 6
7. INDICATION/OPERATION PANEL ........................................................................................................... 7
7.1
7.2
7.3
Name and description of each component of indication/operation panel ........................................... 7
Function and indication of indication/operation panel........................................................................ 8
General operation of indication/operation panel ................................................................................. 9
8. CALIBRATION ........................................................................................................................................... 10
8.1
8.2
8.3
8.4
8.5
8.6
8.7
Kinds of standard gas ........................................................................................................................ 10
Preparation of standard gas ............................................................................................................... 10
Calibration concentration setting (except zirconia O2 sensor) .......................................................... 12
Calibration concentration setting (zirconia O2 sensor) ..................................................................... 14
Zero calibration (air point calibration in case of zirconia O2 sensor) ............................................... 16
Span calibration (low concentration point calibration in case of zirconia O2 sensor) ...................... 17
Auto calibration ................................................................................................................................. 18
9. OPERATION ............................................................................................................................................... 25
9.1
Operating procedure .......................................................................................................................... 25
– vi –
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10. MAINTENANCE ......................................................................................................................................... 26
10.1 Routine maintenance and inspection................................................................................................. 26
10.2 Periodic maintenance and inspection ............................................................................................... 28
10.3 Other maintenance and inspection .................................................................................................... 28
10.4 Concentration guarantee term of standard gas cylinder (for NOx, SO2, CO and O2 analyzer) ......... 29
10.5 Maintenance of sampling device ....................................................................................................... 29
10.6 Maintenance of zirconia O2 sensor.................................................................................................... 35
10.7 Others, major component figures ...................................................................................................... 35
11. STANDARD ACCESSORIES AND SPARES ........................................................................................... 36
11.1 Standard accessories.......................................................................................................................... 36
11.2 Spares for 1 year (optional) ............................................................................................................... 37
12. PROCESSING OF HEATING PIPE ENDS ................................................................................................ 38
12.1 Outline ............................................................................................................................................... 38
12.2 End processing method ..................................................................................................................... 39
12.3 Check after piping ............................................................................................................................. 41
12.4 Clamp support ................................................................................................................................... 41
12.5 Specifications of tube trace ............................................................................................................... 42
12.6 Specifications of heating pipe ........................................................................................................... 42
13. TROUBLESHOOTING ............................................................................................................................... 43
13.1 Troubleshooting of instrument .......................................................................................................... 43
13.2 Error codes and remedies .................................................................................................................. 44
14. SPECIFICATIONS ....................................................................................................................................... 45
CODE SYMBOLS ............................................................................................................................................... 49
SAMPLING SYSTEM BLOCK DIAGLAM ...................................................................................................... 50
OUTLINE DIAGRAM......................................................................................................................................... 52
CONNECTION DIAGRAM ................................................................................................................................ 53
– vii –
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1. OUTLINE
The infrared gas analyzer (ZSP) can continuously and accurately measure the concentration of gases such as NOx,
SO2, CO, CO2 and O2 contained in the flue gas from a stationary generating source. The analyzer is available in
both single-component and multi-component types depending on customer’s specification. The actual analyzer
may somewhat differ from the descriptions in this manual depending on the specifications demanded by each
customer. For outline diagram, piping system, hardware configuration, specifications, standard accessories, spares
and supplies, refer to the delivery specifications submitted individually.
Note: For details of the infrared gas analyzer, refer to the instruction manual INZ-TN2 ZRG separately
prepared.
2. SPECIFICATIONS
Please refer to Chapter 14. Specifications. Note that the contents of the separately issued data sheet have priority.
3. COMPOSITION
(1) Gas sampling section
(2) Gas piping
1 set (depending on customers’ designation)
1 set (depending on customers’ designation)
1
(3) Accommodation locker
Infrared gas analyzer ZRG
Zirconia O2 sensor ZFK 3, 4
Converter ZDL
1 or 2 (depending on customers’ designation)
1 (depending on customers’ designation)
1 (for NOx measurement)
Sampling
1 set
Standard gas, pressure regulator
Standard accessories
1 set (depending on customers’ designation)
1 set
Spares and supplies for 1 year
1 set (depending on customer’s designation)
– 1 –
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4. INSTALLATION
Danger
• This product is not explosion-proof. Do not use it in explosive gas-rich atmosphere. Otherwise, serious
accidents such as explosion and fire may be caused.
Caution
• Installation, carrying and relocation must be made by a qualified contractor or your dealer.
Incorrect installation results in falling accidents, electric shocks or fire accidents.
• The gas analyzer is heavy. Special care should be taken for installation to prevent trouble or injury due
to falling or dropping of the analyzer.
• When the gas analyzer needs to be lifted, be sure to put on gloves. Do not hold it with bare hands to
prevent injury.
• This product must be installed in a place that meets the conditions specified in the ‘instruction manual.’
Use in a place that is outside the given installation conditions may cause an electric shock, fire or mal-
function.
• During installation work, attention should be paid not to allow entrance of wire fragments, etc. into the
product. Otherwise, a fire, trouble or malfunction may be caused.
There are a number of conditions which must be met for operating the gas analyzer stably over a long time.
4.1 Selection of installation site
A site which satisfies the following conditions should be selected for installation of the analyzer.
(1) A place which is near the gas sampling location
(2) A place which is not exposed to direct sunlight or heat radiated from a high temperature object (One
which is not exposed to rain or water splash in case of indoor type)
(3) A place which has a clean atmosphere (dust and corrosive gas not present)
(4) A place with a minimum of vibration
(5) A place where daily variation in temperature is minimum
4.2 Selection of gas sampling location
A place which satisfies the following conditions should be selected.
(1) A typical place where the gases to be analyzed exist
(2) Where the gases always flow without stagnation
(3) A place easy of access for maintenance and inspection
(4) Where the gases respond quickly to a change in the process operating conditions
(5) Where variation in pressure, temperature, etc. is minimum
– 2 –
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4.3 Installation work
For installation of the analyzer locker and the extractor, follow the piping instructions in Fig. 4-1 and the
separately issued approval drawings (outline diagrams, sampling system diagram).
(1) Countermeasures for cold climate
(a) Freeze prevention of gas piping
(b) Freeze prevention of drain pot
(c) Freeze prevention of bypass and drain pipes
(2) Countermeasurement for vibration
When installing in a place where vibration is considerable, the locker should be floated on antivibration
rubber pads.
4.4 Connection of cables
Caution
• Request an installation company or your dealer to carry out wiring.
If wiring is incomplete, shock hazard or injury may be caused.
• Class D grounding construction is mandatory. Otherwise, shock hazard may be caused.
<Caution for wiring company>
For preventing shock hazard, fire and injury, be sure to observe the following.
• Before wiring, be sure to turn off the primary power supply. If this is neglected, you may receive and
electric shock.
• For grounding, use a 600 V-IV wire having diameter of 2 mm2 or more and an adequate dielectric
strength.
• Connect the power supply which meets the rating of product. Connection of other power supply may
cause a fire.
• Select the diameter of input and output wires, which matches the rated current of gas analyzer.
• Be sure to use solderless terminals for connection to the input and output terminal block.
• Use the terminal block for branching the output wire.
• Be sure to fix the input and output wires onto the floor, wall surface, etc. and use a protective device for
wires.
The lead-in for AC power cables and outlet for signal wires are provided at the bottom of the analyzer or else
at the specified place. Connect AC power cables and output signal wires according to the separately issued
wiring diagrams.
Note: Avoid connecting the analyzer power supply near devices such as high-frequency heating fur-
nace or electric welder which greatly disturb the power waveform, and avoid sharing the same
power lines with such devices. Class D grounding construction (100W ground resistance) is
required.
4.5 Connection of pipes (refer to piping instructions in Fig. 4-1 and separately issued approval
drawings)
(1) Connect gas pipe between the gas extractor and the analyzer inlet (sample gas inlet). Use a joint, etc.
for ø10/ø8 Teflon pipe when connecting to ensure there will be no leakage.
(2) Additionally tighten the joint section if necessary
– 3 –
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Fule
(Note 1)
300 or
more
Gas extractor
ZBAK
Note)
Vertical
300
Horizontal
installation
(Note 2)
Sampling
pipe
Leave 300mm space for inspection
and exchange of filter.
Gas outlet facing downward (or horizontal)
Use termination kit TFC-7HPT-10JM (Note 6) or
caulk with silicone bolding agent, etc. after
insulation of heater wire (for indoor installation).
Mating flange for
installing extractor
JIS 5K 65A FF
*
Radius 300mm
or more
Heater power supply
100V AC
* Supporting wire
Gradient of 15˚
or more (Note 4)
Teflon pipe φ10/φ8 or tube trace
(heating pipe) SE-10C1-56-1-PVC-M
or equivalent.
Outer sheath for Teflon pipe ø10/ø8 is
PVC and bundle outer sheath is ø33.
* Support
For pipe end processing, refer to Section 12.
(Note 3)
Peel off covering
by about 2m.
(φ10/φ8 teflon tube
inside heating pipe)
(Note 7)
Power connection kit
TFC-3HPT-10JM (Note 6)
Gas
conditioner
Direct lead-in
Filter
*
Gas
conditioner
(in panel)
(Note 7)
Gas analyzer
Sample tube
(Note 5)
60 × 120 square
hole for wiring
*Exhaust
+ Drain
Drain
Drain
Drain
* Drain port (Note 8)
Front-view diagram
The part marked by the asterisk is not supplied.
Fig. 4-1 Piping procedure
Note 1) To prevent aspiration of leaked air
Note 2) Install so that pipe end comes to nearly center of flue and is at right angle to the gas flow.
Note 3) Peel off heating pipe by about 2m in order to air-cool measured gas.
Note 4) Provide an inclination of 15° or more on the gas pipe so that drain will not accumulate in the event
of power failure, etc.
Note 5) Exhaust and drain share the same output. In the case of indoor installation, provide a drain pot
and carry out drain separation, and exhaust air outside (pipe inner diameter should be ø8 or
more).
Note 6) Use this when utilizing a heating pipe. (Maker : Fujikin, Japan)
Note 7) The gas pipe (ø10/ø8 teflon tube) should be inserted directly into the gas conditioner.
Note 8) In outdoor application or in a cold district, protect the drain pot and pipes with a heat insulating
material, etc. to prevent drain from freezing in winter.
– 4 –
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5. DESCRIPTION OF EACH PART
Please refer to Chapter 14 specification attached at the end of the manual.
6. PREPARATION FOR OPERATION
6.1 Injection of clean water
Inject clean water through the filter or air aspiration port until it overflows from the gas conditioner.
6.2 Supply of external power
Supply external power to the analyzer. And check the connections with output signal wire, etc. The exter-
nal power supply should be.........
100V±10% AC,
50/60 Hz ±1%,
with power consumption of 0.9kVA max. (excluding heating pipe).
Check with reference to the separately issued approval diagrams.
6.3 Check of sample piping, exhaust piping, etc.
Check the connection of the sample piping and if necessary, provide exhaust piping + drain piping (Pipes
with inner diameter of ø8 or more for both). When sample will be dispersed upward, then branch and water-
seal the exhaust pipe for the purpose of drain separation. Be sure to disperse the exhaust into the atmo-
sphere.
Make checks with reference to the piping instructions in Fig. 4-1 and the separately issued gas analyzer
diagram.
– 5 –
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6.4 Airtightness test
(1) Piping inside panel
Since airtightness is confirmed during tests before shipment, an Airtightness test during trial run is
usually unnecessary. When a long time has passed after shipment, then carry out the following proce-
dure.
(a) Close the drain port.
(b) Connect standard gas to the sample gas inlet.
(c) Connect the transparent tube of the conditioner air suction port (see Fig. 10-1) vertically (in place
of a manometer).
(d) Flow standard gas gradually, and after reaching a pressure of about 1961Pa, close the needle valve
of the pressure regulator.
(e) Check the water level at the air suction port of the conditioner, and if the drop in the level in less
than 147Pa/min, then the error due to insufficient airtightness is negligible.
(f) If a leak is present when measuring a harmful gas, make a check by applying soapy water to the
normal pressure section while aspirating outside air.
(2) Piping outside panel
Thoroughly check the tightened condition of pipe joints. If necessary, apply pressure from the extrac-
tor outlet side and make a test as in the preceding item (1).
(3) If the airtightness is insufficient, make a test on each section, find the faulty location and make it
completely airtight. If the faulty location is before the aspirator, then air enters the gas pipe midway to
cause a drop in the indication.
6.5 Setting of temperature inside locker
Turn on power supply to a space heater depending on the ambient temperature. Ventilation fan should
always be turned ON.
6.6 Warm-up time
Turn ON the auto breaker.
(1) Gas extractor
Turn ON the power switch and warm up the extractor for at least 1 hour.
(2) Heating pipe (option)
Turn ON the power supply auto breaker of heating pipe and warm up the pipe for at least 1 hour.
(3) Electronic gas cooler
Turn ON the power switch and warm up for at least 10 minutes.
(4) NO2/NO converter (option)
Turn ON the switch, set the temperature regulator at 220°C, and warm up for about 30 minutes until
indication of the temperature reaches 220±2°C. 200°C for a NO/CO (+ O2) analyzer
(5) Analyzer
Turn ON the power switch and carry out warm-up.
Infrared gas analyzer: about 8 hours
Zirconia O2 sensor: about 30 minuets
– 6 –
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7. INDICATION/OPERATION PANEL
7.1 Name and description of each component of indication/operation panel
3
4
5
6
Unit indication lamp
Day indication
Sub indication
Range changeover switch
2
1
Main indication
Component indication
SU TU TH SA
MOWE FR
Vol%
ppm
RANCE
NOX
SO2
Vol%
ppm
RANCE
RANCE
Vol%
O2
HEAS
CAL SET
SET
HOLD
RANCE
AUTO SAL
CAL
7
Function indicator lamp
FUNC COMP
ENT
ZERO
SPAN
8
9
Function key
Component selector key
15 Calibration start key
14 Span calibration key
13 Zero calibration key
12 ENT key
10 Digit shift key
11 Numeric input key
(Three component of NOx, SO2 and O2 are indication in this figure.)
Part Name
Description
q Component indication
w Main indication
Indicates kind of gas measured.
Indicates measured concentration. Also indicates various set-points for alarm function, auto
calibration function (option), etc.
e Unit indication lamp
r Day indication
Indicates units of measured gas concentration.
Indicates current day or day of starting by means of bar in auto calibration (option) setting mode.
Indication SU
MO
TU
WE
TH
FR
SA
Day Sun. Mon. Tue.
Wed. Thu. Fri.
Sat.
t Sub indication
Indicates measuring range, error code, various set points, etc.
Used when changing the range. High range is set when pressing and low range is set when
pressing
y Range changeover key
.
u Function indicator lamp
MEAS:
Relevant lamp lights up when following functions are set.
Lights up in measuring status.
CAL SET:
Flashes in calibration concentration setting mode.
ALM SET:
Flashes in alarm setting mode.
HOLD:
Flashes in hold setting mode or lights steadily while hold function is activated.
Flashes in remote range setting mode or light steadily while remote range function is activated.
RMT RANGE:
AUTO CAL:
Flashes in auto calibration setting mode or lights steadily while auto calibration function is
activated.
i Function key
Setting mode is changed at each press of this key (Refer to Section 5).
Set component is changed for each setting mode.
o Component selector key
!
!
!
!
!
!
0
1
2
3
4
5
Digit shift key
Shift is made from highest toward lowest digit at each press of this key.
Selected digit is incremented at each press of this key.
Numeric input key
ENT key
By pressing this key after setting, the set contents are memorized and becomes valid.
Used for zero point calibration. (Lamp flashes in zero calibration mode.)
Used for span calibration (Lamp flashes in span calibration mode.)
Start key for manual calibration. Zero is calibrated by pressing ZERO and CAL keys.
Span is calibrated by pressing SPAN and CAL keys. (CAL lamp lights steadily during calibra-
tion).
Zero calibration key
Span calibration key
Calibration start key
– 7 –
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7.2 Function and indication of indication/operation panel
This panel consists of the following functions.
Key
Function
Main indication
Measuring value
Sub indication Function indication lamp
FUNC
Measuring mode
Range
MEAS lamp lights
Setting mode
FUNC
FUNC
FUNC
FUNC
FUNC
FUNC
FUNC
FUNC
FUNC
FUNC
FUNC
Calib.conc.setting
Calb.conc.
Range
CAL SET lamp lights
ALM SET lamp flickers*
HOLD lamp flicker
Alarm setting (option)
Hold setting
Alarm value
ON or OFF
ON or OFF
Day
Remote range setting (option)
Current time setting
RMT RANGE lamp flickers*
Auto CAL lamp flickers
AUTO CAL lamp flickers
AUTO CAL lamp flickers
AUTO CAL lamp flickers*
AUTO CAL lamp flickers*
AUTO CAL lamp flickers
*
Hr.min.
Auto clib.start time setting
Auto calib.cycle setting
Calib. gas flow time setting
Calib. gas flow time setting
Auto calib.changeover
Key lock changeover
HR.min.
Day
Time
Time
Mode No.
ON or OFF
ON or OFF
ZERO
ZERO
Zero calibration
Span calibration
Measured value
Measured value
Range
Range
Zero key indication flickers
Span key indication flickers
• When the setting mode is assumed, the analog output signal is held at the value just before entering this mode.
• When optional functions are not provided, the contents of these functions are not indicated.
* Refer to the instruction manual of the infrared gas analyzer for the items marked by the asterisks.
– 8 –
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7.3 General operation of indication/operation panel
The measuring mode is assumed when
power is turned ON. The gas concentra-
tion appears on the main indication, while
the range being used appears on the sub in-
dication.
NO
Gas concentration
indication
Range
indication
Advice on Operation
Hige rang is selected
when key is pressed
LWhen selecting the range
In the setting status, as shown in the figure
at the right, the high range is selected when
key is pressed, while the low range is
selected when key is pressed.
Low rang is selected
when
key is pressed
LWhen selecting the gas component
In the setting status, as shown in the figure
at the right, the gas component can be set
by pressing COMP key.
1st component
2rd component
3rd component
Example: When COMP key is pressed
while the 1st component is flash-
ing, the flashing moves to the
2nd component (figure at right).
The setting for the 2nd compo-
nent is now changeable.
COMP
ENT ZERO SPAN CAL
* The 1 component type analyzer is not pro-
vided with COMP key.
Pressing changes the settable gas component.
ZERO SPAN
LFor releasing zero or span
If a mistake has been made in zero or span
calibration, then perform a reset in the fol-
lowing way.
Pressed wrongly.
ZERO SPAN
The figure at the right shows an example.
If SPAN key has been pressed mistakenly
instead of ZERO key, then press SPAN
key again. Calibration is released.
The lamp blinks.
ZERO SPAN
Press again to extinguish the lamp.
Thus reset. Press the
key afresh.
ZERO
If ZERO key has been pressed mistak-
enly instead of SPAN key, the press
ZERO key again.
Calibration is released.
– 9 –
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8. CALIBRATION
Danger
• When handling standard gas such as calibration gas, read the instruction manual for the standard gas for
correct handling. Special care should be taken when handling hazardous gas such as CO gas and the like
to prevent poisoning.
8.1 Kinds of standard gas
8.1.1 When not using zirconia O2 sensor
(1) Zero gas: N2 or atmospheric air/instrument air depending on specification (when without verifi-
cation stipulated in the laws for measurement and weighing)
(2) Span gas: Gas of 90% or more full scale for each component, remainder is N2 (span gas for low
range will be delivered unless otherwise specified)
8.1.2 When using zirconia O2 sensor
(1) Zero gas: Air (Span gas of the O2 analyzer in the laws for measurement and weighing).
(2) Span gas: 1 to 2% O2, remainder is N2. (Zero gas of the O2 analyzer in the laws for measurement
and weighing).
Gas of 90% or more full scale for other than zirconia O2 sensor, remainder is N2.
Note: For separately calibrating the low and high ranges of the zirconia O2 sensor, supply 9 to
10% O2 and the remainder N2 for the low range (10%) and use air for the high range
(25%).
8.2 Preparation of standard gas
The standard gas to be used for calibration is delivered in a separate package from the locker.
Check the kind of standard gas to be used according to the sampling system diagram, and set it at the
prescribed location.
Before starting calibration, attach a pressure regulator to the standard gas.
8.2.1 How to mount pressure regulator for standard gas cylinder
(1) Before mounting a pressure regulator to the gas cylinder, clean the gas cylinder adapter. Entry of
dust into the pressure regulator may result in gas leaks.
(2) If packing is not inserted in the mounting nut for the cylinder or it is damaged, replace it with
supplied spare one.
(3) Use a spanner of a proper size, fasten the cylinder mounting nut to the gas cylinder. Mount
supplied joint to the outlet according to Item “Sampling system block diagram”.
(4) Loosen the pressure controls and then tighten the outlet controls.
(5) Open a valve of the gas cylinder, and the pressure gauge on the high pressure side indicates a
pressure of the gas cylinder by flowing gas into the pressure regulator.
(6) Turn the pressure controls clockwise to increase the secondary pressure; adjust the pressure con-
trols so that a pressure gauge on the low pressure side reads 30 kPa.
(7) Open the outlet controls to release gas.
– 10 –
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Adapter
Pressure gauge on
high pressure side
Pressure gauge on
low pressure side
Pressure controls
Packing
Cylinder mounting nut
Pressure regulator
Cylinder
R1/4 joint
Output handle
Fig. 8-1 Pressure regulation for standard gas cylinder
– 11 –
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8.3 Calibration concentration setting (except zirconia O2 sensor)
Set a span value for the calibration concentration setting. (Zero point calibration concentration is fixed at
zero.)
Set the calibration gas concentration (span value).
NO
When FUNC key is pressed in the measuring sta-
tus, the previously set span value will appear on
the main indication.
FUNC
The CAL SET LED of the function indicating
lamps will flicker.
NO
By pressing the
key, the highest digit of the
main indication for the 1st component will flicker,
and the span value can not be set.
CAL SET
Select a range with the
keys.
NO
NO
NO
After selecting the range, set a span value in this
status.
The numeric value will be incremented by press-
ing
key.
The digit to be set can be selected by pressing
key.
ENT
For selecting the 2nd and subsequent compo-
nents and the range, press the
key and
while the main indication for the 1st compo-
nent is flickering, press the COMP key and
then the main indication for the component to
be set will flicker. Now press the
select the range to be set.
keys to
When the span value has been set, press the ENT
key. Setting operation is completed.
– 12 –
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[When adjusting for each range]
(Simultaneous calibration of H and L ranges has been factory-set).
Perform setting in the following way.
NO
By pressing CAL key while the highest digit of the
main indication for the 1st component is flickering,
CAL
then ‘
’ will appear on the main indication and
‘ ’ will appear on the sub indication.
NO
NO
NO
Press
key and will change to
.
= Meaning of set values =
: The calibration is valid only for the selected
range, and zero and span calibration can
be made independently for each range.
By conducting zero and span calibration
for one range, the calibration will be done
automatically for the other ranges as well.
ENT
:
When the selection has been finished, press the ENT
key. Setting operation is completed.
– 13 –
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8.4 Calibration concentration setting (zirconia O2 sensor)
A zirconia O2 sensor sets the zero (air) point (span point stipulated in the laws for measurement and
weighing) of the O2 analyzer. For the density of calibration gas to be used, refer to “8.2 Preparation of
standard gas”.
LSetting of calibration concentration for zero (air)
point (zero stipulated in the laws for measurement
and weighing)
By pressing the FUNC key in the measuring status,
O2
the calibration concentration previously set for the zero
(air) point will appear on the main indication.
FUNC
The CAL SET LED of the function indicating lamps
will flicker.
O2
By pressing the
key, the higher digit of the main
indication of the O2 analyzer will flicker and zero point
setting is enabled.
CAL SET
Press the
keys to select a range.
O2
O2
O2
The numeric value will be incremented by pressing
key. The digit to be set is selected by pressing the
key.
Setting ranges are 20.2 to 21.9 Vol. % for high
range and 7.0 to 21.9 Vol. % for law range.
ENT
Set the air concentration for both high and low
range.Note)
Press the ENT key after setting the zero point. Set-
ting operation is completed.
Note: When using air for the high range and 9 to 10 Vol. % O2/N2 for the low range, set the density
for each range.
When viewing from the zirconia O2 sensor side, the air point corresponds to the zero point.
Therefore, calibration should begin with the air point.
Also, since the air point and low concentration point can be calibrated by the zero calibra-
tion key and span calibration key, respectively, the air point and low concentration point
are regarded as the zero and span in this manual.
– 14 –
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LSetting of span calibration concentration (zero point
stipulated in the laws for measurement and weigh-
ing)
Setting of each component
Press the CAL key in the status where the digit of the
O2 analyzer main indication is flickering via the zero
(air) point calibration concentration setting.
O2
CAL
The previously set span value will now appear on the
main indication.
NO
The ‘CAL SET LED’ of the function indicating lamps
COMP
will flicker.
O2
O2
O2
Then, press the COMP key and the highest digit of
the 02 analyzer main indication will flicker and the
span value is now settable.
Press the
keys to select a range.
When the range has been selected, set a span value in
this status.
ENT
The numeric value will be incremented by pressing
the
key.
Press the
lected.
key and the digit to be set can be se-
Press the ENT key after setting the span value. Set-
ting operation is completed.
– 15 –
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8.5 Zero calibration (air point calibration in case of zirconia O2 sensor)
This is used for adjusting the zero point.
Flow the zero gas (0.3N/min.) by adjusting the needle
valve of pressure regulator and wait until the indica-
tion stabilizes.
When the Zirconia O2 sensor is used, use air.Note)
NO
NO
ZERO
When the indication has stabilized, select the measur-
ing range to be calibrated by using the
keys.
Flickers
When using a multi-component analyzer, all the
components undergo zero calibration simulta-
neously at the selected range.
ENT ZERO SPAN CAL
CAL
ZERO
Press the ZERO key, and
flicker.
key lamp will
NO
Lights
Next press the CAL key and conduct zero calibra-
tion.
ENT ZERO SPAN CAL
CAL
The
key lamp lights steadily during calibra-
ENT ZERO SPAN CAL
tion.
( Lamp is turned off after calibration )
Since the measuring status is resumed after the cali-
bration, carry out the calibration for other ranges if
necessary.
Note: When using different gases for the low and high ranges, apply 9 to 10 Vol. % O2/N2 which has
been set for the low range.
When the function for automatic calibration is provided, the solenoid valve turns on and cali-
bration gas flows upon pressing the ZERO key.
– 16 –
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8.6 Span calibration (low concentration point calibration in case of zirconia O2 sensor)
Carry out span calibration by flowing calibration gas at
the concentration set as a span value.
NO
Flow the calibration gas (0.3 N/min.) by adjusting the
needle valve of pressure regulator. Wait until the indica-
tion stabilizes, and then conduct span calibration.
SPAN
SPAN
Press the SPAN key and the
key lamp flickers.
NO
Flickers
In the case of a multi-component analyzer, the main
indication will flicker for the components which
can be calibrated.
ENT ZERO SPAN CAL
(
)
COMP
Press the COMP key and the settable gas compo-
nent will change.
When the gas component has been determined,
NO
press the
keys and select a range.
Note: The lamp will not flicker in the case of a
single-component analyzer.
Flickers
ENT ZERO SPAN CAL
(In case of a multi component analyzer)
Next press the CAL key and conduct span calibration.
CAL
CAL
The
key lamp lights steadily during calibration.
NO
Since the measuring status is resumed after calibration,
continue the calibration for each component and each
range.
lights
ENT ZERO SPAN CAL
ENT ZERO SPAN CAL
( Lamp is turned off after calibration )
Note: On the low range of zirconia type O2 sensor, when zero gas is calibrated with 9 to 10 Vol. % O2,
the zero and span calibrations interfere with each other. So, each calibration should be re-
peated a few times.
When the function for automatic calibration is provided, the solenoid valve turns on and the
span gas for the selected component flows upon pressing the SPAN key.
– 17 –
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8.7 Auto calibration
In this analyzer, the signals form the input/output terminals on the upper can be used for driving an external
solenoid valve and introducing standard gas, whereby zero point and span can be calibrated automatically.
The auto calibration is done according to 8.7.1 Current time setting, 8.7.2 Auto calibration start time setting,
8.7.3 Auto calibration cycle setting, 8.7.4 Auto calibration ON/OFF setting and 8.7.5 Output Hold setting at
Calibration.
Cautions on operation
1. When the auto calibration start time is reached during key operation, the auto calibration is given
priority and is started. All key operation will be invalid until the auto calibration is finished.
2. To forcibly interrupt the auto calibration in progress, press both the ENT and CAL keys simulta-
neously. After the forcible interrupt, the measuring mode is resumed and all the keys are operable.
Although the current auto calibration will be passed over, it will be started from the initially set
cycle from the next time onward.
Example: When auto calibration is set for 3 hour intervals starting from 8:00 a.m.
: Under auto calibration
8 : 00
11 : 00
14 : 00
17 : 00
8 : 00
11 : 00
14 : 00
17 : 00
Forcible interruption
3. Key operation is possible while calibration is not under way with the auto calibration function set.
Therefore all settings (of span, hold, remote range, time, etc.) including manual calibration can be
made. But note that if the wrong time is set on the clock, the auto calibration will not be started at
the correct time.
4. Auto calibration is able to start by applying remote start input signal, 5V DC longer than 100msec,
to remote start input terminals. In this case, auto calibration will start independent to its ON/OFF
setting. (Calibration starts at the trailing edged of signal.)
5. When measuring 4 components, or NOx, SO2, CO and O2 (with 2 infrared gas analyzers), the auto-
matic calibration cycle should be set on the CO/O2 analyzer side and the automatic calibration of
NOx/SO2 analyzer should be turned OFF. After the automatic calibration of CO/O2 analyzer, the
automatic calibration of NOx/SO2 analyzer will be started.
– 18 –
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Example of auto calibration time chart for 4-component measurement
Auto calibration start time
Under
Under auto calibration
measurement
Zero
gas
Span
gas 1
Zero
gas
Span
gas 1
Span
gas 3
Substi-
tution
Span
gas 2
Span
gas 3
SO2
CO
O
2
NO
O
2
Gas flow time
•
•
Auto calibration
gas flow time
T
T
T
T
T
T
T
T
T: settable from 100 to 599 sec. (Note)
Auto calibration cycle
Gases introduced:
Sample gas
Zero gas
Span gas 1
CO
Span gas 1
NO
Span gas 2
SO2
Span gas 3
O2
Indicator lamps
AUTO CAL.
•
Flickers
ZERO
SPAN
CAL
Flickers
Lights
HOLD
(at HOLD ON)
Auto calibration abnormality:
If an abnormality occurs during auto calibration, a contact signal for auto calibration abnormality will be
output from the input/output terminals on the upper of the analyzer. The gas which incurred the abnormality
will not be calibrated, and instead the next component will be calibrated.
Note: Usually, T is set at 360 sec. for measurement including SO2, and at 180 sec. for other measurements.
For change of setting, refer to the separate instruction manual of infrared gas analyzer.
– 19 –
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8.7.1 Current time setting
Set the current time and day of the week.
FUNC
Press the FUNC key in the measuring status.
The AUTO CAL LED of the function indicating lamps
will flicker.
SU TU TH SA
MO WE FR
NO
The main indication shows the hour and minute via a
24-hour indication and the decimal point flickers.
A’–’ bar lights up at the relevant weekday on the sub
indication.
AUTO CAL
Flickers
(
)
SU TU TH SA
NO
NO
NO
Indication SU MO TU WE TH FR SA
MO WE FR
Day
Sun. Mon. Tue. Wed. Thu. Fri. Sat.
key and the time is now settable.
(
)
Press the
SU TU TH SA
The highest two digits of the main indication will flicker.
MO WE FR
ENT
The numeric value is incremented by pressing the ‘
’.
SU TU TH SA
MO WE FR
Press the
key and the digit can be selected.
After the time setting, press
on the sub indication.
key and the day is settable
The bar indication will flicker.
Press the
key and the bar will shift.
Press the ENT key when the time and day setting is fin-
ished. The data are saved.
Time starts from the point where ENT key is
pressed.
– 20 –
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8.7.2 Auto calibration start time setting
When FUNC key is pressed at the current time indica-
tion, the auto calibration start time and day will appear on
the main and sub indications.
SU TU TH SA
MO WE FR
NO
Lights
The AUTO CALLED of the function indicating lamps
will flicker. In the case of start time, the decimal point on
the main indication will light steadily.
FUNC
SU TU TH SA
MO WE FR
NO
Press the
key and the auto calibration start time is
AUTO CAL
settable, so set a start time on the main indication.
(
)
The numeric value is incremented by pressing the
key.
SU TU TH SA
NO
NO
NO
MO WE FR
Press the
key and the digit can be selected.
(
)
SU TU TH SA
After setting the calibration start time, press the
key
and the calibration start day can be set on the sub indica-
tion.
MO WE FR
ENT
The bar indication will flicker.
SU TU TH SA
MO WE FR
Press the
key and the bar will shift.
The auto calibration start time is settable up to one
week ahead.
When the auto calibration start time and day have been
set, press the ENT key. The data are saved.
When the auto calibration at the set time is fin-
ished, the next auto calibration start time will be
set automatically.
To confirm the next auto calibration start time, then
carry out this operation and check the indication.
Note: When the auto calibration start time has been set, then set the auto calibration cycle.
– 21 –
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8.7.3 Auto calibration cycle setting
The calibration cycle is settable in either ‘days’s or ‘hours’.
Press the FUNC key at the calibration start time indica-
NO
NO
tion and ‘
’ will appear.
FUNC
The AUTO CAL LED of the function indicating lamps
will flicker.
Press the
The highest digit on the sub indication will flicker. Select
either ‘days’ or ‘hours’ by pressing the key.
key and the auto calibration cycle is settable.
AUTO CAL
(
)
‘ ’ appears on the sub indication when selecting
‘days’ and ‘ ’ appears when selecting ‘hours’.
NO
NO
NO
(
)
Press the
key and the calibration cycle and be set in
the lower digits of the sub indication.
The numeric value is incremented by pressing the
key.
ENT
Press the
key and the digit can be selected.
Day is settable in a range of 1 to 7 days. Hour is
settable in a range of 1 to 99 hours.
Note
If ‘0 0’ (hours) is set, it will be automatically set
to ‘1’(hours).
Press the ENT key when the calibration cycle has been
set. The data are saved.
– 22 –
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8.7.4 Auto calibration ON/OFF setting
Select whether or not to carry out auto calibration.
’ when calibration will not be made.Note)
NO
NO
Set to ‘
Press the FUNC key at the calibration gas flow mode
indication and ‘ ’ will be appear.
FUNC
The AUTO CAL LED of the function indicating lamps
will flicker.
AUTO CAL
Press the
be set.
key and auto calibration ON or OFF can
Select either ‘
’ or ‘
’ on the sub indication by
NO
NO
NO
pressing the
key.
When the auto calibration ON/OFF setting is finished,
press the ENT key. Setting operation is completed.
ENT
Note: In case of 4-component (NOx, SO2, CO and O2) analyzer, be sure to turn OFF the automatic
calibration of NOx/SO2 analyzer.
– 23 –
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8.7.5 Setting of output hold at calibration
This is used when calibrating for holding the output sig-
nal at the value just be before entering calibration. (The
indication is not held.)
The hold function is settable for each component.
FUNC
Press the FUNC key in the measuring status and
NO
‘
’ will be indicated.
HOLD
The HOLD LED of the function indicating lamps will
flicker.
Press the
key and the hold function will be settable.
NO
NO
NO
The sub indication will flicker.
Select hold ‘
’ or ‘
’ by pressing the
key.
Press the ENT key after setting the hold function. Set-
ting operation is completed.
ENT
Setting is valid for all the components.
At hold ON, the HOLD of the function indicating lamps
will light steadily while the hold function is activated.
At hold OFF, these lamps will go off.
In case of automatic calibration, output is held while the
automatic calibration lamp is lit.
In case of manual calibration, output is held for about half
an hour after completion of calibration.
For canceling the output hold forcibly, turn off the hold
setting once.
Note 1: When measuring 4 components, or NOx, SO2, CO and O2 (with 2 infrared gas analyzers),
output is held by using the external hold function at the time of automatic calibration.
Note 2: In the setting mode, output is held indifferently to the ON/OFF status of hold setting.
Note 3: In case the analyzer is equipped with a maintenance switch, output is held while the switch
is turned on.
– 24 –
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9. OPERATION
Danger
• If you notice malodor or abnormal sound, stop the instrument immediately. If this is neglected, fire may
occur.
Caution
• When the analyzer is to be operated after it has been left unused for a long time, the operating procedure
is different from the normal stop/start procedure. It should be handled according to the procedure shown
in the instruction manual to ensure its proper performance and to prevent trouble or injury.
• Do not operate the analyzer for a long time with its door left open to avoid entry of dust into the analyzer.
Dust deposits will result in damage to the analyzer.
Prohibition
• Do not insert a rod or your finger into the fan (electronic cooler at ceiling), otherwise injury may be
caused by the rotating blades.
• Do not touch metal, finger, etc. to the input and output terminal block of analyzer. Otherwise, shock
hazard or injury may be caused.
• Smoking and use of fire/flame is prohibited in the vicinity of the gas analyzer. Otherwise, a fire may
occur.
• A water-filled container such as a bucket should not be placed on the roof of the gas analyzer having
indoor specifications. If such a container turns over, spilled water may cause shock hazard or burning
inside the analyzer.
9.1 Operating procedure
(1) Check if all the preparation for operation have been completed.
(2) Press the range selector switch on the indication/operation panel to select a range to be used.
(3) Press the function key “FUNC” on the indication/operation panel to light up the “MEAS” function
indicator lamp.
(4) Turn on the aspirator power supply and confirm that the ball of flow meter is at 0.4N/min.
Prescribed flow rate may be 0.5N/min. So it should be checked in the piping system diagram sepa-
rately presented.
– 25 –
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10. MAINTENANCE
Danger
• When handling standard gas such as calibration gas, read the instruction manual for the standard gas for
correct handling. Special care should be taken when handling hazardous gas such as CO gas and the like
to prevent poisoning.
• During maintenance or inspection, be sure to turn ON the ventilation fan in the analyzer to prevent
poisoning due to gas leakage.
• When the gas filter of the analyzer is to be replaced or the washing unit needs maintenance, be sure to
close the calibration gas valve. Especially, if the calibration gas valve is located at the sample gas inlet,
the replacing or washing shall be done after closing the calibration gas valve to prevent poisoning or
other trouble.
Caution
• The gas converter is heated to about 220°C. When the catalytic agent needs to be replaced, turn OFF the
power for the converter and use heat-proof gloves about 30 minutes later.
• When the fuse is blown off, check the cause of it and replace it with the same type of fuse having the
same capacity to prevent electric shocks or other trouble.
• When the analyzer is provided with a power leak relay, press the test button to confirm proper operation
before making maintenance or inspection to prevent electric shocks.
• Be sure to lock the door. Do not allow unauthorized persons to use the door key. Do not touch the door
carelessly to prevent electric shocks and other trouble.
The following items must be observed to prevent electric shocks or injury and to ensure safety.
• Take off metallic objects such as wrist watch before starting the work.
• Do not touch the device with wet hands.
10.1 Routine maintenance and inspection
Maintenance/inspection item
Procedure
Monitoring of sample flow rate
Monitoring of conditioner bubbling quantity
Prescribed flow rate: The flow rate is normal when the ball is at
0.4N/min. and there is slight bubbling at the bottom of conditioner.
Adjust the needle valve so that a flow rate of 0.4N/min. is available.
If the prescribed flow rate is unobtainable even with the needle valve
fully open though there is slight bubbling, then the capillary (sample
line) should be checked for clogging. In case there is no bubbling, the
aspirator, conditioner, electronic cooler and pipe should be checked for
clogging. And if water decreases in the conditioner because of heavy
bubbling, the capillary of bypass line should be checked for clogging.
(Note)
Good if H2 level shown in Fig. 10-1 is longer than 100mm.
If air is aspirated through the air aspiration tube, then the pressure loss at
the stage before the conditioner filter has become large. Check the gas
extractor filter (see (1) in 10.5) and gas pipes for clogging.
Conditioner
Air aspiration tube level
– 26 –
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Maintenance/inspection item
Procedure
Contamination of membrane filter
Replace the filter paper if it has blackened (see (3) in 10.5).
If contamination occurs rapidly, then check the pre-stage filters of the
gas extractor ((1) in 10.5), conditioner filter ((2) in 10.5), etc.
Electronic gas cooler
Check the fan rotation.
Temperature controller for NO2/NO converter Check that the controlled temperature is approx. 220°C (200°C in case
of NO/CO analyzer).
Note) Bubbling will be eliminated when a pressure control valve is equipped.
Prescribed flow rate value should be checked in the piping system diagram separately presented.
Conditioner filter
O-ring (G65)
Fastening nut
Wing bolt
Sample gas
To analyzer
Water
injection
Aspirator
Upper chamber
Electronic
gas cooler
Air
aspiration
pipe
H2
Capillary
or
Pressure
control valve
Bypass
Capillary
H1
H1: Sample negative pressure
Exhaust after analysis
H2: Good when longer than 100mm.
Be careful when within 50 to 100mm.
Check extractor filter piping when
shorter than 50mm.
Lower chamber
Drain and exhaust
Slight bubbling
(Bubbling is eliminated when
the unit is provided with
pressure control valve.)
Fig. 10-1 Conditioner
– 27 –
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10.2 Periodic maintenance and inspection
Maintenance/inspection item
Analyzer calibration
Referential frequency
Weekly
Procedure
Refer to section 8.5 to 8.6.
Check of standard gas filled
pressure
It takes at least 1.5 months to deliver the standard gas. So
the gas should be ordered 2 or 3 months in advance.
Water level in upper chamber of
conditioner
Monthly
Every two months
Biannually
Supply water if level is below overflow port.
Replacement of membrane filter
paper
Replace with new filter paper (stop the aspirator when
exchanging). See 10.5 (3).
Inspection and replacement of
conditioner filter, O-ring
Replace these parts if flow rate doesn’t increase because of
adherence of dust. See 10.5 (2).
Capillary
Replace if clogged.
Check of valve and diaphagm of
aspirator (pump)
Check and clean diaphragm. Use valve by turning it to 90°
rightward (replace valve when it is turned once). See 10.5
(4).
Leak test of pressure regulator
Replacement of standard gas
Apply soapy water or the like and check for bubbles. Either
retighten or replace packings if necessary.
NO, SO2, CO/N2 of less than 250 ppm. See 10.4.
Replacement of gas extractor filter
element, O-rings
Yearly
O-ring requires replacement. Filter element may be reusable
after cleaning. See 10.5 (1).
Catalyst of NO2/NO converter
Replacement (when NO2 gas concentration is 10 ppm or
less)
Note: Replace once every 8 months when NO gas con-
centration is measured in the setting range of 0 to
200ppm or more at 0.5L/min.
Replacement of standard gas
Aspirator
See 10.4.
Replacement of diaphragm
Clean pipes or replace if necessary.
Contamination, leak test of piping
Exchange of water in conditioner
Overhaul
10.3 Other maintenance and inspection
(1) Space heater and ventilating fan
If the ambient temperature drops below 5°C during winter or the like, then turn ON the space heater.
The ventilating fan should always be left ON.
(2) Blowback of gas extractor (option)
Turn off the aspirator and close the measured gas line before conducting a blowback. Frequent blowback
will cause the temperature of the gas sampler to drop and result in corrosion, so it should be kept to a
minimum.
– 28 –
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10.4 Concentration guarantee term of standard gas cylinder (for NOx, SO2, CO and O2 analyzer)
Kind of gas
NO/N2
NO/N2
SO2/N2
SO2/N2
CO/N2
CO/N2
O2/N2
Concentration range
0.4ppm or more, and less than 250ppm
250ppm or more, and less than 5%
0.4ppm or more, and less than 250ppm
250ppm or more, and less than 1 %
2.4ppm or more, and less than 100ppm
100ppm or more, and less than 15%
0.9% or more, and less than 25%
—
Guarantee term
6 months
1 year
6 months
1 year
6 months
1 year
1 year
N2
*None
Air
—
*None
* Schedule the use for about one year under proper control.
Note: It is empirically known that standard gas concentration remains within the adequate accuracy
for 6 months or 1 year. However, gas maker’s guarantee term is as listed in the above table.
Therefore, replacement is required within the guarantee term when importance need be placed
on traceability.
10.5 Maintenance of sampling device
(1) Replacement of filter element of gas extractor (extractor type : ZBAK1)
(a) Turn off power supply to the extractor
(b) Turn off the pump of gas analyzer
(c) After making sure the temperature of extractor has dropped adequately, detach the rainproof cover
(remove the wing bolt on the flange side).
(d) Remove the locking wing bolt and pull out the internal parts while gripping the handle for filter ex-
change.
Although you may feel slight stiffness in pulling out the handle for filter exchange, it should be pulled
out gradually while turning it.
(e) Remove the metallic mesh filter from the seal fixture.
(f) After mounting a new element, reverse the above procedure.
Locking wing bolt
Seal fixture
Filter case
Handle for filter exchange
O-ring
(JIS P48A Viton)
Metallic mesh filter
Fig 10-2 Gas extractor (type ZBAK1)
– 29 –
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(2) Replacement of mist filter element (See Fig. 10-1.)
(a) Loosen the butterfly bolt, and pull the head up and out of the container.
(b) Then loosen the retaining nut and remove the contaminated filter element.
(c) Replace with a new conditionor filter and O-ring, and reassemble by reversing the above steps.
(3) Replacement of membrane filter element
(a) Turn off the power to the gas aspirator (pump).
(b) Turn the lid of the membrane filter counterclockwise and remove it.
(c) After removing the lid, detach the inner O-ring and replace the filter element.
(d) Wipe dust out of the case by using a clean cloth. Be careful not to let dust enter the gas outlet side.
(e) After replacing the filter, reassemble by reversing the above steps.
(f) Attach the flouro pour filter closely to the filter supporting bracket.
(g) Apply vacuum grease about once every 6 months to the O-ring.
Filter element
Lid
Inner O-ring
Outer O-ring
Case
Supporting bracket (used with fluoro-pour filter)
Fig. 10-3 Membrane filter
– 30 –
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(4) Replacement of the valve and the diaphragm of diaphragm type aspirator
Replace the seat valve (turn 90° in six months and replace annually) and the diaphragm (replace annually)
according to the following procedure.
(a) Turn off the power supply of the aspirator and
remove the inlet and outlet piping connected to
the aspirator.
(b) Remove the four hexagon socket head cap
screws. Then cap A and cap B are separated
and the valve can be removed.
Hex. socket head
cap screw
(c) Turn the diaphragm counterclockwise with your
hand and remove it.
Cap A
(d) Place a new diaphragm to the position and mount
it by turning it clockwise until it stops.
Note) When mounting, check that the dia-
phragm is securely engaged in the
screw section of the arm slot. Other-
wise malfunction may result.
Rc1/8
Seat valve
Cap B
(e) Place the valve on cap B and turn it 90∞. Check
that the notches of cap A and cap B are aligned,
and then tighten the four hexagon socket head
cap screws.
Diaphragm
Note) Since complex valve seat is adopted, re-
move the pin on the underside of the
valve from the hole to which the pin has
been inserted and reinsert it to the
other hole.
Arm lot
(f) Turn on the power of the aspirator in the inter-
face module. Check that it does not generate
abnormal sound. Check also with your hand that
the valve is normally operated, that is, air is as-
pirated from the IN side and discharged from
the OUT side. If any abnormality is observed,
repeat the procedure from the beginning.
(g) After checking that the aspirator is normally op-
erated, turn off the power of the aspirator in the
interface module, and return the piping to the
original position.
Fig. 10-4 Exploded view of diaphragm type aspirator
Note) Do not apply force abruptly to Rc1/8
screw part when returning the piping
to the original position.
– 31 –
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(5) Check and maintenance of electronic gas cooler
(a) Fan motor
This motor should be replaced periodically every 20,000 hours (about 2 years in case of continuous
operation ) as a standard though this varies with operating condition. However, if no abnormality
cannot be found at the time of a periodic replacement, the motor is further usable continuously.
(b) Gas passage cleaning procedure
When bubbling has come to diminish significantly, it can be thought that the passage has come to be
clogged by dust, etc.
In this case, the gas passage needs be cleaned in the procedure given below.
(i) When looking at the inside of INLET joint, area B of the
INLET joint
spiral guide can be seen. In the area B, a lateral hole of
C
1.5mm dia. is bored. So, insert the top of the furnished
OUTLET
INLET
spiral pull-out device into the hole as shown below and
extract the spiral guide.
(ii) Clean the gas passage and spiral guide. For detergent,
use a one having a chemical composition which will not
affect hard glass, hard PVC, polyethylene and fluoro-
rubber. After washing, rinse adequately with water and
dry the inside well by blowing compressed air.
B
Spiral pull-out
device
Spiral guide
Heat exchanger
(iii) When inserting the spiral guide to the original position,
it should be pressed lightly until area A of the spiral guide
comes in contact with the bottom. As a standard, area B
of the spiral guide should be located with a distance L of
about 15 to 20mm from the top face C of INLET joint.
Note that attention should be paid since piping is stepped.
A
Note) For sampling with the pressure control valve, clean
the gas passage using the above procedure when
the sample flow begins to be extremely reduced.
DRAIN
Fig. 10-5 Structure of electronic dehumidifier
– 32 –
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(6) Replacement of NO2/NO converter catalyst
(a) Turn off power supply to the converter.
(b) After half an hour, remove q w e, and extract r
upward and downward, respectively. Pay attention
not to suffer a burn. In addition, carefully handle the
ceramic pipe for preventing breakage. When remov-
ing r , e will fall simultaneously. So prepare a
catalyst receiver.
q Connection
rubber
Ring
w
e Filter
r Catalyst
Filter
e
t
Fastener
(c) Wind glass wool on the tip of r and insert it from
the bottom together with q. Inject one pack of new
catalyst from the top. Set w e on the top side. (This
step is unnecessary when a membrane filter is pro-
vided at the later stage.)
Ceramic
pipe
y
q Connection
(d) Connect the pipe, set the temperature controller at
220°C (200°C for NO/CO analyzer), and turn on
power supply.
rubber
Fig. 10-6 Structure of NO2 /NO converter
(7) Setting of temperature controller for NO2/NO converter (PXZ4)
(a) When pressing the PV/SV key, display changes over between PV and SV. (Usually, PV (Process
Variable) display is set).
(b) Under SV (Set Value) display, set 220°C by pressing the
key. (200°C need be set for NO/CO analyzer.)
or
key and determine it by the ENT
(c) Parameter need not be set because they have been factory-set.
(d) The temperature controller controls converter temperature through the SSR relay.
(8) Setting of pressure control valve
The pressure control valve has been set the discharge about 2 N/min. of sample gas together with drain,
when the pressure at the inlet is about 50 kPa. The set pressure increases with a right turn of the setting knob
and decreases with a left turn.
Do not turn the setting knob unless the sample flow needs to be changed.
Setting knob
2-Rc1/4
Sample
OUT
IN
Fig. 10-7 External appearance of pressure control valve
– 33 –
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(9) Washing the Permapure dryer
The Permapure dryer is used for SO2 measurement (2000 ppm or more).
The Permapure dryer has no moving sections nor consumable parts. If precautions in using it are suffi-
ciently respected, it can operate without maintenance usually. However, if its element has clogged, for
example, remedy it by the following method.
Purge IN
Header
Element tube
Purge joint
Shell joint
Sample
OUT
Sample
IN
Shell
Sample joint
O ring presser
Tee
Purge OUT
O ring
Fig. 10-8 Structure of Permapure dryer
(a) Disassembly
q Remove an O ring presser (one side).
w Loosen a shell joint (one side).
e Push the header inward and remove the tee.
r Loosen the other shell joint and gently pull out the element.
(b) Washing
q Carry out washing with tap water (detergent, alkali solution not allowed).
w On a side, remove the sample joint, cap and tee.
e Through the opposite port and purge port, introduce tap water at 127 kPa or lower pressure and
300 to 500 mN/min of flow rate.
r Carry out washing for longer or shorter time according to the degree of clogging.
If the clogging is slight, approximately 1 hour of washing is enough.
Tap water
Tap water
Element tube
Permapure dryer
Fig. 10-9 Washing of Permapure dryer
– 34 –
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10.6 Maintenance of zirconia O2 sensor
Sensor temperature
OXYGEN ANALYZER
800
POWER
ON
1
2
3
4
5
6
7
OFF
+
–
AG
0V
ALM
Power SW Fuse 3A Terminal
Front view
Sample inlet Outlet (Rc 1/4)
(Rc 1/4)
Side view
(1) Appearance of zirconia O2 sensor
(2) Routine maintenance
No parts require periodic maintenance. In case sensor temperature is 800±5°C or the SO2 concentration in
sample gas is high, you should check occasionally that the outlet pipe is not clogged by the precipitation of
crystal. Because the sample outlet is at a high temperature, attention should be paid not to suffer a burn.
10.7 Others, major component figures
Rc1/4
Gas outlet
Up
2-Ø4.5
mounting holes
19
Mounting direction
Ø20 panel cutout
Gas intlet
Rc1/4
34
5
31
Approx. 25 (when fully open)
– 35 –
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11. STANDARD ACCESSORIES AND SPARES
Caution
• Do not use replacement parts which are not specified by makers. Use of these parts will not only
provide the required performance but also result in damage or other trouble.
• Replacement parts used for maintenance must be handled as incombustible objects.
11.1 Standard accessories
Quantity (analyzer)
No.
Part name
Type of part No.
Remarks
NOX/SO2 NOX
SO2
—
2
Other
1
2
Membrane filter paper
TK701837C6
TK741833P3
—
1 pack
1 pack 25 sheets per pack
Flouro pour filter for
membrane filter
2
—
—
3
4
5
Fuse (for instrument switch) Various types
2 each 2 each 2 each 2 each For 2A, 3.2A
Cooler puller
Joint
—
1
1
1
1
TK7F7627P1
1 set
1 set
1 set
1 set
Measuring number of gases + 1
For pressure regulator
6
Hose band
TK539474C410
100% 100% 100% 100%
For ø6 tube
For pressure regulator
7
8
9
Toalon tube 0.3m
Polyethylene tube 1m
Anchor bolt
TK727528P1
415966P4
1
1 set
4
1
1 set
4
1
1 set
4
1
1 set
4
For ø6 tube
ø6/ø4 For standard gas
Option
M12 x 160 x 50
10 Instruction manual
INZ-TN2ZSP
INZ-TN2ZRG
1
1
1
1
11 Analyzer accessories
1 set
1
1 set
1
1 set
1
1 set
1
Infrared analyzer fuse 2A x 2pcs.
Cell cleaning cloth x 1pc.
O2 analyzer fuse x 1pc.
12 Wash bottle
TK7H3493P1
For conditioner
Note) Part No. 8 will be shipped in connection with the solenoid valve in the locker.
– 36 –
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11.2 Spares for 1 year (optional)
Quantity (analyzer)
No.
Part name
Spare for converter
Remarks
TK726889C3
NOX/SO2 NOX
SO2
—
2
Other
1
2
3
4
5
6
7
8
Note 2)1
1
2
—
2
Catalyst and filter
TK7H8043P1
Conditioner filter
2
2
Conditioner O-ring
2
2
2
G65 chloproprene 8553765
25 sheets of TK701837C6 per pack
TK741833P3
Membrane filter paper
Fluro pour filter for membrane filter
Membrane filter rubber ring
Membrane filter O-ring
Capillary
—
6
1
pack
—
1
—
6
1
pack
—
1
1
1
Chloroprene
G65 chloroprene
For 0.5 K
TK733572P1
8553765
1
1
1
1
1
—
1
—
(only when with pressure control valve)
9
Capillary (for bypass)
1
1
1
1
1
1
1
1
TK729264C6 (ø1mm)
(only when without pressure control valve)
10 Capillary (for cooler out)
TK729264C7 (ø1.4mm)
(only when without pressure control valve)
11 Aspirator diaphragm
12 Aspirator valve
1
1
1
2
1
1
1
2
1
1
1
2
1
1
1
2
TK725417P5
TK725417P6
When gas extractor is
simultaneously supplied.
(ZBAK1)
13 Gas extractor filter element
TK7H8439P1
85504N3
14 Gas extractor O-ring
P48A
Note 1) The contents of standard accessories, and spares and supplies for 1 year may vary somewhat
according to the specifications.
Note 2) Two parts are required when flow rate is 0.5N and NO range is beyond 200 ppm.
Code for preparation of 1-year spares and supplies
Analysis gas
NOx, SO2, (CO), (O2)
Same as above
NOx, (CO), (O2)
Same as above
SO2, (O2)
Extractor
With
Code
Remarks
ZBN4SP12
ZBN4SP22
ZBN4SP32
ZBN4SP42
ZBN4SP52
ZBN4SP62
ZBN4SP72
ZBN4SP82
SO2 meter range 200 to 1000ppm
SO2 meter range 200 to 1000ppm
Without
With
Without
With
SO2 meter range 200 to 1000ppm
SO2 meter range 200 to 1000ppm
Same as above
CO, (O2)
Without
With
Same as above
Without
– 37 –
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12. PROCESSING OF HEATING PIPE ENDS
12.1 Outline
(1) Configuration
Power supply 100VAC, 50/60Hz
Power connection kit
About 2000
Heating pipe
Termination kit
About 500
Fig. 12-1
(2) Caution on connection of heating pipe
q
The clearance between clamp supports must be about 1.2 m in the horizontal direction and about 3 m in
the vertical direction.
w
For a bent piping, bending should be moderate enough to ensure a minimum bending radius of 300 mm
or more.
Clamp support
No good
Good
Fig. 12-2
(3) Connection diagram
A heater wire is wound around 2 isolated buses and it is brought into contact with the buses alternately at
intervals of 300 mm (heating unit).
Power supply
Heating wire
300mm
300mm
300mm
300mm
300mm
300mm
Fig. 12-3
– 38 –
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12.2 End processing method
(1) Power supply side (power connection kit)
q
w
When cutting out the heating pipe, take care not to damage the heater wire.
Pulling out on the inside of grid section provides a non-heating area of about 300 mm at maximum.
Grid
Non-heating area of 300mm long
Fig. 12-4
e
Peel the outer sheath covering of heater as shown below and cut off the heater wire as close to its root
as possible.
(HTP type heater has fiber glass, heater wire and thin Teflon covering under its outer sheath covering.
So the outer sheath covering should be peeled neatly.)
115 mm
Cut off at root.
Fig. 12-5
r
Apply RTV (silicone sealant) to the terminal boots and plug the boots into the heater. Then wind a
sealing tape across the boots and heater.
RTV
RTV
Terminal boots
10
Fig. 12-6
t
For connection with the power supply wire, use a press-fitting sleeve. If the press-fitting section is
loose, contact resistance becomes large to cause abnormal heating of the sleeve.
Fig. 12-7
– 39 –
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(2) Termination side (termination kit)
q
Cut the heater in the dimension shown at right.
Grid
Grid
Push back the metallic braiding and fix it with
Teflon tape.
40mm
300mm
w
Peel the outer sheath covering of heater and cut
off the heater wire as close to the root as pos-
sible. Expose the bus of heater wire toward the
cut end starting from a point about 40 mm away
from the nearest grid. (HTP type heater has fi-
ber glass, heater wire and thin Teflon covering
under its outer sheath convering. So the outer
sheath covering should be peeled neatly.)
150 mm
Grid area
Outer sheath
covering
Metallic
braiding
Teflon tape
Inner sheath covering
Outer sheath covering
12mm
e
r
Cut off buses at different lengths.
Bus
Cut off at root
Heater wire
Wind Teflon tape while carefully securing isola-
tion between the heater wire and buses.
6mm
Outer sheath covering
Inner sheath covering
Teflon tape
t
Apply RTV silicone sealant to the end cap and
the Teflon tape-wound section. Then, fit the end
cap while bleeding air.
RTV silicone sealant
Note) After fitting the cap, move it back
slightly.
Fit while turning
End cap
Seal tape
y
Fix the end cap by winding seal tape as many
times as possible for preventing the cap from slip-
ping off.
Note) Never short-circuit the end (bus) of
heater.
– 40 –
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12.3 Check after piping
q
w
e
r
t
y
The heating pipe is not sunk significantly due to a clamp, etc.
The bent section has an adequately large bending radius.
Electrical connections are exact.
The end of heater wire (bus) is not short-circuited (it must never be short-circuited).
All parts of the connection kit (sealing connector), etc. have been used.
Screws of the connection kit (sealing connector), etc. have been tightened completely.
12.4 Clamp support
Clamps for conduit should be used. For heating pipe profile of the tube trace, refer to 12.5.
The heating pipe should be clamped so that it will be sunk significantly.
No good
Good
Fig. 12-8
– 41 –
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12.5 Specifications of tube trace
(1) Structure of tube trace
1
4
Heater cable
PFA teflon
3
2
5
q
w
e
r
t
Heater cable (power limiting cable)
Process tube
Aluminum tape
Fiber glass heat insulator
PVC jacket
Fig. 12-9
(2) Specifications of tube trace
q
w
e
r
t
Heater cable
Process tube
Aluminum tape
Fiber glass
HPT 20-1 BN 35.4w/m at 100ºC (100V AC)
10/8 mm øPFA Teflon tube
50% overlap
Thermal conductivity 0.2kJ/m·h·ºC
UL 105ºC, black PVC
PVC jacket
12.6 Specifications of heating pipe
Maker: Thermon Far East
Dealer: Fujikin, Japan
– 42 –
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13. TROUBLESHOOTING
Caution
• When trouble cannot be remedied even after following the instruction manual, contact your dealer or
Fuji's service station (serivice engineer). Do not disassemble the device, as it results in electric shocks
or injury.
13.1 Troubleshooting of instrument
Trouble
Decrease of sample Filter (primary, second-
gas flow rate ary, tertiary filters)
Probable location
Check item
Remedy
Check if filter element is clogged.
Clean or replace element.
Diaphragm type aspirator Check if aspirator is working normally.
Check for abnormal sound or vibration.
Clean or replace.
Retighten screws or replace
aspirator.
Electronic gas cooler
Check if cooler is working normally,
check cooling temperature and check for
clogging of flow path.
Clean or replace.
Conditioner
Gas leakage
Flowmeter
Water decreases in lower chamber.
Inject water and check the
capillary (bypass).
Check for gas leakage in piping after
aspirator or at joints.
Retighten or replace parts.
Check for accumulation of drainage or
dust in flowmeter. Check adjustment of
needle valve.
Clean the flowmeter.
Adjust needle valve.
Piping, capillary
Check for bent or clogged piping.
Check for capillary.
Replace.
Increase of bubbling Bypass flow path
Clean or replace.
Connect properly.
Disassemble and clean.
flow rate
Piping
Check for deviated joint.
Rise of sample gas
Pressure control valve
Pressure control valve is clogged.
flow
(Note)
Indicated value is
abnormal.
Gas leakage
Check for gas leakage in parts before
aspirator such as secondary coarse filter
holder, piping, joints, etc.
Retighten or replace parts.
Diaphragm
type aspiration
Check if aspirator is normally operating
and sample gas is flowing at set value.
Clean aspirator or replace
parts such as diaphragm or
value
Adjust sample gas flow.
Conditioner
Check if water level is normal.
Check if air is aspirated.
Supply water.
Check primary filter.
Dissolution of gas
Sampling pipe
Check for accumulation of drainage in
piping.
Clean, and tilt piping so
drainage does not accumulate.
Check if SUS pipe is used (for SO2
analyzer).
Change to teflon tube.
Note) Pressure control valve is used.
– 43 –
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Trouble
Probable location
Gas leakage
Check item
Remedy
Check for gas leakage before the
aspirator.
Retighten or replace parts.
Indicated value is
not as expected.
Interference due to
moisture
With respect to zero gas indication, the
indicated value when air is introduced
exceeds ±2% full scale.
Readjust to compensate for
moisture interference.
Measuring range
Zero, span
Check if correct range is set.
Reset the range.
Check zero and span using standard gas. Adjust for correct zero
point and span.
Cell window
Check if cloudy
Clean the window.
Replace the fuse.
Power supply, fuse
Check the power supply voltage and fuse.
Indication doesn’t
change
13.2 Error codes and remedies
This analyzer is provided with self-diagnosis functions, and an error code is displayed if an abnormality
occurs in the instrument.
Take a proper measure with reference to the instruction manual of infrared gas analyzer when an error code
appears.
– 44 –
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14. SPECIFICATIONS
Specifications
Type of cubicle:
Outdoor, self-standing, sealed type or indoor type
Non-dispersion infrared absorption (NDIR method) for NOx, SO2, CO and CO2;
zirconia method for O2.
Measuring system:
Sampling system:
Measuring range:
Dry sampling electronic cooling & dehumidification system
(Permapure dryer adopted)
NOx — 0 to 100 .... 2000 ppm
SO2 — 0 to 100 .... 1000 ppm
(Range selection:
Max. rate 1:20
(except for O2))
CO — 0 to 200 .... 2000 ppm
CO2 — 0 to 5 ........ 50%
O2 — 0 to 10/25%
Note: Measuring range of each gas is 50 to 5000ppm, available in
approved type (special order).
Repeatability:
Drift:
±0.5% of full scale
Zero — ±2% of full scale/week for NOx, SO2 and CO
±2% of full scale/month for O2
Span — ±2% of full scale/week
Linearity:
±2% of full scale
Response time:
90% response from the inlet of cubicle
SO2 : 4 min. CO : 2.5 min NO : 2 min
Others : 3 min.
Output:
4 to 20mA DC (allowable load resistance 550Ω), non-isolated.
For the number of output points, see Table 1.
Contact output:
Indication:
Each NO (1a) contact (100V AC, 1A) for error (analyzer error, calibration error) and
auto calibration status
Digital indication (indicating measured value and measuring range on analyzer front
panel of infrared gas analyzer)
Sample gas extracting rate: Approx. 2 N/min.
Gas extractor:
Electrical heating type (filter built in)
Filter mesh — 40µm mesh of 316 stainless steel
Probe
— 316 stainless steel, length 600, 800 or 1000mm
— JIS 5 K65AFF
Flange
Sample inlet tube:
ø 10/ ø 8mm teflon tube for CO and O2 meter and NOx and O2 meter
Heating tube ( ø 10/ ø 8mm teflon tube) for NOx, SO2 and O2 meter and NOx, SO2, CO
and O2 meter
Standard gas (3.4 N):
Standard air gas for zero calibration and O2 span calibration
Standard analyte/remaining N2 gas for low range span calibration and O2 zero calibration
Form for all components already approved
Form verification:
Ambient temperature:
Power supply:
-5 to +40°C
100±10V AC, 50 or 60Hz
Power consumption:
Mass (weight):
Approx. 1,200 VA (excluding consent and heating tube)
Approx. 300 kg (excluding standard gas)
Finish color:
Munsell 5Y 7/1 semigloss
– 45 –
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Standard requirements
for sample gas:
Temperature —
60 to 800°C
— 100 mg/Nm3 or less
2.94 to +2.94kPa
Dust
Pressure
—
-
Components — SO2 0 to 1000ppm
NOx 0 to 2000ppm (NO2 100ppm or less)
CO2 several % to over 10%
CO 0 to 2000ppm
O2 0.5 to 21%
H2O 0 to 40%
HCN 0 to 100ppm
N2 remaining percent
When other components are contained in the sample gas, consult with Fuji.
Note) NO2/NO converter catalyst life:
1 year/NO2, 10ppm
1 month/NO2, 100ppm
Installation requirements:Select a location free from direct sunlight and severe vibration.
Table 1 Number of output points and kinds of outputs
Type
ZSP1L
ZSP1F
ZSP1P
ZSP1B
CO, O2
ZSP1A
ZSP1H
ZSP1M
Measuring
component
NOx, SO2,
CO, O2
NOx, SO2,
O2
NOx, O2
SO2, (O2)
NOx, CO2, O2
NOx, SO2,
CO, CO2, O2
No. of
11
7
3
3
3
5
12
output points
Kind of output A, B, C,
A, B, D, E,
A, D, E
C, D, K
B, (D)
A, B, D, E, K
A, B, C,
D (2 points), E, F, H, J
D (2 points),
E, F, G, H, J,
K, L
F, G, H, J, K
A: NOx instantaneous value
C: CO instantaneous value
B: SO2 instantaneous value
D: O2 instantaneous value
E: NOx instantaneous value after O2 correction
G: CO instantaneous value after O2 correction
J: 1hr. moving average SO2 value after O2 correction
L: O2 instanteneous value
F: SO2 instantaneous value after O2 correction
H: 1hr. moving average NOx value after O2 correction
K: 4hr. moving average CO value after O2 correction
– 46 –
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(1) NOx after O2 correction
CO after O2 correction
(a) Calculating equation
21 - On
C=
• Cs
21 - OS
C: Concentration after O2 conversion
Cs: NOX or CO concentration measured
Os: O2 concentration measured
On: O2 concentration as conversion basic:
4% Oil combustion boiler
5% Gas combustion boiler
6% Solid object combustion boiler, petroleum heating furnace
12% Garbage incinerator
(b) Block diagram
NOx or
CO signal
O
2/NOx conversion
21 - On
21 - Os
· Cs
or CO (ppm)
Zurconia
type O2 sensor
O
2
O
2
converter
signal
Full scale is the same as
instantaneous value before
conversion.
Infrared gas analyzer
(2) Moving average output
1 hr. moving average output (for NOx, SO2)
4 hr. moving average output (for CO)
– 47 –
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Automatic calibration
• Calibration tolerance:
±0.2% FS
• Automatic calibration output hold: Possible
(Example in 4 component analyzer):
CO zero
CO span
O2
zero
NOx, SO2 zero
NOx span
SO2 span
O2
span
Automatic
calibration
• Calibration cycle:
• Calibration gas feed time:
• Display:
Once/day (variable, up to 7 days)
2 to 10 min. (variable), common to each gas
Calibration failure
Error code (E-) is displayed when one-time calibration volume is more
than ± 20% FS on both zero and span and it is under calibration:
CAL lamp ON
Ordering information
1. Measuring range of analyzer
2. Length of sampling pipe
3. Insertion length of sampling tube
4. Power voltage/frequency
5. Instruction required when standard gas is not necessary
6. Instruction required when individual inspection is not necessary
7. Necessity of spares and supplies (for 1 year)
8. Additional functions
Note: When special functions such as remote range selection, output hold by external contact, auto-
matic calibration, automatic calibration start by external contact, insulation output, measured
value concentration alarm, etc. are required, they should be separately designated.
– 48 –
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CODE SYMBOLS
1
Z
2
S
3
P
4
5
6
7
8
4
9 10 11 12
Descrption
Application
Combustion exhaust gas (standard condition)
Other exhaust gas
1
2
Component
NOX + (O2
)
P
A
B
F
CO + (O2
)
SO2 + (O2
)
NOX + SO2 + (O2
)
NOX + SO2 + CO + (O2
NOX + SO2 + CO + (O2
Others
)
)
H
L
Z
Oxygen analyzer
Without
With ZFK
0
1
3
With ZKG (Non-standard)
Auto calibration
1
With
Type of cubicle
Indoor installation type
Outdoor installation type
1
2
External piping
Heating pipe
ø10 Teflon tube
1
2
Standard gas
3.4r
10r
3.4r + instrument air
10r+ instrument air
3.4r + atmopheric air
10r+ atmopheric air
1
2
3
4
5
6
Power supply
100V AC/50Hz
100V AC/60Hz
Others 50Hz
5
6
9
0
Others 60Hz
– 49 –
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SAMPLING SYSTEM BLOCK DIAGLAM
– 50 –
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Functions of individual components
• Gas extractor (type; ZBA):
With heating type stainless steel filter; standard diameter 40µm for filter.
• Gas conditioner (type; ZBH9)
For separating drain and removing sulfuric acid mist and oil mist or fine dust particles. Besides, for
preventing aspiration of drain at clogging of extractor filter or sampling pipe, and activating composite
operation of constant-pressure bubbler for maintaining a constant sample supply to analyzer.
• Aspirator (type; ZBG8)
For aspirating sample gas (sample gas flow rate: about 2N/min.)
• Electronic gas cooler (type; ZBC)
An electronic dehumidifier which dries the moisture in sample gas to a dew point of aproximately 2°C.
• Converter (type; ZDL):
Added to the NOx analyzer. A converter using a special catalyst which converts NO2 gas into NO. The
catalyst must be renewed annually (built in the temperature regulator).
• Solenoid valve (type; AB21)
Used for the introduction of calibration gas.
• Memberane filter (type; ZBBM)
Eliminates fine dust particles with glass-fiber or flouropore filter, and permits monitoring dust adher-
ing condition on the front of the body.
• Flow meter (type; ZBD)
Ajusts and monitors standard flow rate of sample gas.
• Standard gas (type; ZBM):
Reference gas used for calibrating zero and span of the analyzer. When using a zirconia oxygen meter,
this is used together with air for calibrating zero for NO, SO2, and CO and for calibrating span for O2.
• Zirconia O2 sensor (type; ZFK3, 4)
Used in combination with the infrared analyzer. Outputs about 0V at measurement of the air, and an
inverse logarithm of about 1V at measurement of 0.05% O2.
• Pressure control valve (type; ZBD35)
Sample gas pressure is controlled to 49kPa to maintain a constant flow rate.
– 51 –
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OUTLINE DIAGRAM (Unit:mm)
For outdoor installation type
Anchor plan and door opening
diagram
1000
815
620
Cable inlet (60 × 120
Rear
side
rectangular hole)
with plastic resin-
cover (PVC)
Rc 3/8
Front
side
A-140-2-1
(key No.200)
Anchor bolt (option)
( 4 – M12 × 160 × 50 )
Rc 1/2
760
800
620
800
4-φ15 hole
For indoor installation type
Anchor plan and door opening
diagram
800
800
620
Cable inlet (60 × 120
Rear
side
rectangular hole)
with plastic resin-
cover (PVC)
Rc 3/8
Front
side
A-140-2-1
(key No.200)
Anchor bolt (option)
( 4 – M12 × 160 × 50 )
850
Rc 1/2
760
800
620
800
4- φ15hole
– 52 –
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CONNECTION DIAGRAM
1
L1
L2
G
Power supply
100V AC
2
3
4
5
J1
J2
Extractor
6
7
H1
H2
A1
A2
A3
A4
B1
Heating tube
8
9
NOx instantaneous value
NOx average value
SO2 instantaneous value
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
B2
B3
SO2 average value
B4
C1
O2
instantateous value
C2
C3
NOX instantateous value
SO2 corrected value
C4
C5
C6
C1A
C2A
E1
O2
instantateous value
CO instantaneous value
CO average value
E2
E3
E4
C7
CO corrected value
C8
D11
D12
D21
D22
Failure contact output
On maintenance and auto
calibration contact output
Note: Terminal numbers are fixed.
(only specified outputs are wired).
– 53 –
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Head Office
Gate City Ohsaki, East Tower, 11-2, Osaki 1-chome,
Shinagawa-ku, Tokyo 141-0032, Japan
Instrumentation Div.
International Sales Dept.
No.1, Fuji-machi, Hino-city, Tokyo 191-8502, Japan
Phone: 81-42-585-6201, 6202 Fax: 81-42-585-6187
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