Fuji Labs Welding Consumables ZSP User Manual

Instruction Manual  
INFRARED GAS  
ANALYZER  
TYPE: ZSP  
INZ-TN4ZSPb-E  
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CAUTION ON SAFETY  
Before use, carefully read this “Caution on safety” so that the product is usable correctly.  
• The precautions given here are of great significance to safety. Therefore, they should be observed without fail.  
The precautions on safety are classified into ranks “Danger”, “Caution” and “Prohibition.”  
Danger  
Items which pertains to incorrect handling that may lead to personal death  
or serious injury  
Caution  
Items which pertains to incorrect handling that may lead to medium trouble,  
injury or physical damage  
Prohibition  
Items which pertains to prohibition (DO NOT)  
Installation, carrying, relocation and storage of gas analyzer  
Danger  
• This product is not explosion-proof. Do not use it in explosive gas-rich atmosphere. Otherwise,  
serious accidents such as explosion and fire may be caused.  
Caution  
• Installation, carrying and relocation must be made by a qualified contractor or your dealer.  
Incorrect installation results in falling accidents, electric shocks or fire accidents.  
• The gas analyzer is heavy. Special care should be taken for installation to prevent trouble or injury due  
to falling or dropping of the analyzer.  
• When the gas analyzer needs to be lifted, be sure to put on gloves. Do not hold it with bare hands to  
prevent injury.  
• This product must be installed in a place that meets the conditions specified in the ‘instruction manual’  
Use in a place that is outside the given installation conditions may cause an electric shock, fire or  
malfunction.  
• During installation work, attention should be paid not to allow entrance of wire fragments, etc. into the  
product. Otherwise, a fire, trouble or malfunction may be caused.  
– ii –  
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Caution on wiring  
Caution  
• Request an installation company or your dealer to carry out wiring.  
If wiring is incomplete, shock hazard or injury may be caused.  
• Class D grounding construction is mandatory. Otherwise, shock hazard may be caused.  
< Caution for wiring company >  
For preventing shock hazard, fire and injury, be sure to observe the following.  
• Before wiring, be sure to turn off the primary power supply. If this is neglected, you may receive an  
electric shock.  
• For grounding, use a 600 V-IV wire having a diameter of 2 mm2 or more and an adequate dielectric  
strength.  
• Connect the power supply which meets the rating of product. Connection of other power supply may  
cause a fire.  
• Select the diameter of input and output wires, which matches the rated current of gas analyzer.  
• Be sure to use solderless terminals for connection to the input and output terminal block.  
• Use the terminal block for branching the output wire.  
• Be sure to fix the input and output wires onto the floor, wall surface, etc. and use a protective device  
for wires.  
Caution on use  
Danger  
• If you notice malodor or abnormal sound, stop the instrument immediately. If this is neglected, fire  
may occur.  
Caution  
• When the analyzer is to be operated after it has been left unused for a long time, the operating proce-  
dure is different from the normal stop/start procedure. It should be handled according to the procedure  
shown in the instruction manual to ensure its proper performance and to prevent trouble or injury.  
• Do not operate the analyzer for a long time with its door left open to avoid entry of dust into the  
analyzer. Dust deposits will result in damage to the analyzer.  
– iii –  
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Caution on use  
Prohibition  
• Do not insert a rod or your finger into the fan (electronic cooler at ceiling), otherwise injury may be  
caused by the rotating blades.  
• Do not touch metal, finger, etc. to the input and output terminal block of analyzer. Otherwise, shock  
hazard or injury may be caused.  
• Smoking and use of fire/flame is prohibited in the vicinity of the gas analyzer. Otherwise, a fire may  
occur.  
• A water-filled container such as a bucket should not be placed on the roof of the gas analyzer having  
indoor specifications. If such a container turns over, spilled water may cause shock hazard or burning  
inside the analyzer.  
Caution on maintenance / inspection  
Danger  
• When handling standard gas such as calibration gas, read the instruction manual for the standard gas  
for correct handling. Special care should be taken when handling hazardous gas such as CO gas and  
the like to prevent poisoning.  
• During maintenance or inspection, be sure to turn ON the ventilation fan in the analyzer to prevent  
poisoning due to gas leakage.  
• When the gas filter of the analyzer is to be replaced or the washing unit needs maintenance, be sure to  
close the calibration gas valve. Especially, if the calibration gas valve is located at the sample gas  
inlet, the replacing or washing shall be done after closing the calibration gas valve to prevent poison-  
ing or other trouble.  
Caution  
• The gas converter is heated to about 220°C. When the catalytic agent needs to be replaced, turn OFF  
the power for the converter and use heat-proof gloves about 30 minutes later.  
• When the fuse is blown off, check the cause of it and replace it with the same type of fuse having the  
same capacity to prevent electric shocks or other trouble.  
• When the analyzer is provided with a power leak relay, press the test button to confirm proper opera-  
tion before making maintenance or inspection to prevent electric shocks.  
• Be sure to lock the door. Do not allow unauthorized persons to use the door key. Do not touch the  
door carelessly to prevent electric shocks and other trouble.  
The following items must be observed to prevent electric shocks or injury and to ensure safety.  
• Take off metallic objects such as wrist watch before starting the work.  
• Do not touch the device with wet hands.  
– iv –  
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Others  
Caution  
• When trouble cannot be remedied even after following the instruction manual, contact your dealer or  
Fuji's service station (serivice engineer). Do not disassemble the device, as it results in electric shocks  
or injury.  
• Do not use replacement parts which are not specified by makers. Use of these parts will not only  
provide the required performance but also result in damage or other trouble.  
• Replacement parts used for maintenance must be handled as incombustible objects.  
– v –  
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CONTENTS  
INTRODUCTION ................................................................................................................................................... i  
CAUTION ON SAFETY ....................................................................................................................................... ii  
1. OUTLINE ....................................................................................................................................................... 1  
2. SPECIFICATIONS ........................................................................................................................................ 1  
3. COMPOSITION ............................................................................................................................................. 1  
4. INSTALLATION ........................................................................................................................................... 2  
4.1  
4.2  
4.3  
4.4  
4.5  
Selection of installation site ................................................................................................................ 2  
Selection of gas sampling location ...................................................................................................... 2  
Installation work.................................................................................................................................. 3  
Connection of cables ........................................................................................................................... 3  
Connection of pipes............................................................................................................................. 3  
5. DESCRIPTION OF EACH PART ................................................................................................................. 5  
6. PREPARATION FOR OPERATION ............................................................................................................ 5  
6.1  
6.2  
6.3  
6.4  
6.5  
6.6  
Injection of clean water ....................................................................................................................... 5  
Supply of external power .................................................................................................................... 5  
Check of sample piping, exhaust piping, etc....................................................................................... 5  
Airtightness test ................................................................................................................................... 6  
Setting of temperature inside locker.................................................................................................... 6  
Warm-up time ..................................................................................................................................... 6  
7. INDICATION/OPERATION PANEL ........................................................................................................... 7  
7.1  
7.2  
7.3  
Name and description of each component of indication/operation panel ........................................... 7  
Function and indication of indication/operation panel........................................................................ 8  
General operation of indication/operation panel ................................................................................. 9  
8. CALIBRATION ........................................................................................................................................... 10  
8.1  
8.2  
8.3  
8.4  
8.5  
8.6  
8.7  
Kinds of standard gas ........................................................................................................................ 10  
Preparation of standard gas ............................................................................................................... 10  
Calibration concentration setting (except zirconia O2 sensor) .......................................................... 12  
Calibration concentration setting (zirconia O2 sensor) ..................................................................... 14  
Zero calibration (air point calibration in case of zirconia O2 sensor) ............................................... 16  
Span calibration (low concentration point calibration in case of zirconia O2 sensor) ...................... 17  
Auto calibration ................................................................................................................................. 18  
9. OPERATION ............................................................................................................................................... 25  
9.1  
Operating procedure .......................................................................................................................... 25  
– vi –  
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10. MAINTENANCE ......................................................................................................................................... 26  
10.1 Routine maintenance and inspection................................................................................................. 26  
10.2 Periodic maintenance and inspection ............................................................................................... 28  
10.3 Other maintenance and inspection .................................................................................................... 28  
10.4 Concentration guarantee term of standard gas cylinder (for NOx, SO2, CO and O2 analyzer) ......... 29  
10.5 Maintenance of sampling device ....................................................................................................... 29  
10.6 Maintenance of zirconia O2 sensor.................................................................................................... 35  
10.7 Others, major component figures ...................................................................................................... 35  
11. STANDARD ACCESSORIES AND SPARES ........................................................................................... 36  
11.1 Standard accessories.......................................................................................................................... 36  
11.2 Spares for 1 year (optional) ............................................................................................................... 37  
12. PROCESSING OF HEATING PIPE ENDS ................................................................................................ 38  
12.1 Outline ............................................................................................................................................... 38  
12.2 End processing method ..................................................................................................................... 39  
12.3 Check after piping ............................................................................................................................. 41  
12.4 Clamp support ................................................................................................................................... 41  
12.5 Specifications of tube trace ............................................................................................................... 42  
12.6 Specifications of heating pipe ........................................................................................................... 42  
13. TROUBLESHOOTING ............................................................................................................................... 43  
13.1 Troubleshooting of instrument .......................................................................................................... 43  
13.2 Error codes and remedies .................................................................................................................. 44  
14. SPECIFICATIONS ....................................................................................................................................... 45  
CODE SYMBOLS ............................................................................................................................................... 49  
SAMPLING SYSTEM BLOCK DIAGLAM ...................................................................................................... 50  
OUTLINE DIAGRAM......................................................................................................................................... 52  
CONNECTION DIAGRAM ................................................................................................................................ 53  
– vii –  
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1. OUTLINE  
The infrared gas analyzer (ZSP) can continuously and accurately measure the concentration of gases such as NOx,  
SO2, CO, CO2 and O2 contained in the flue gas from a stationary generating source. The analyzer is available in  
both single-component and multi-component types depending on customers specification. The actual analyzer  
may somewhat differ from the descriptions in this manual depending on the specifications demanded by each  
customer. For outline diagram, piping system, hardware configuration, specifications, standard accessories, spares  
and supplies, refer to the delivery specifications submitted individually.  
Note: For details of the infrared gas analyzer, refer to the instruction manual INZ-TN2 ZRG separately  
prepared.  
2. SPECIFICATIONS  
Please refer to Chapter 14. Specifications. Note that the contents of the separately issued data sheet have priority.  
3. COMPOSITION  
(1) Gas sampling section  
(2) Gas piping  
1 set (depending on customersdesignation)  
1 set (depending on customersdesignation)  
1
(3) Accommodation locker  
Infrared gas analyzer ZRG  
Zirconia O2 sensor ZFK 3, 4  
Converter ZDL  
1 or 2 (depending on customersdesignation)  
1 (depending on customersdesignation)  
1 (for NOx measurement)  
Sampling  
1 set  
Standard gas, pressure regulator  
Standard accessories  
1 set (depending on customersdesignation)  
1 set  
Spares and supplies for 1 year  
1 set (depending on customers designation)  
1 –  
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4. INSTALLATION  
Danger  
This product is not explosion-proof. Do not use it in explosive gas-rich atmosphere. Otherwise, serious  
accidents such as explosion and fire may be caused.  
Caution  
Installation, carrying and relocation must be made by a qualified contractor or your dealer.  
Incorrect installation results in falling accidents, electric shocks or fire accidents.  
The gas analyzer is heavy. Special care should be taken for installation to prevent trouble or injury due  
to falling or dropping of the analyzer.  
When the gas analyzer needs to be lifted, be sure to put on gloves. Do not hold it with bare hands to  
prevent injury.  
This product must be installed in a place that meets the conditions specified in the instruction manual.’  
Use in a place that is outside the given installation conditions may cause an electric shock, fire or mal-  
function.  
During installation work, attention should be paid not to allow entrance of wire fragments, etc. into the  
product. Otherwise, a fire, trouble or malfunction may be caused.  
There are a number of conditions which must be met for operating the gas analyzer stably over a long time.  
4.1 Selection of installation site  
A site which satisfies the following conditions should be selected for installation of the analyzer.  
(1) A place which is near the gas sampling location  
(2) A place which is not exposed to direct sunlight or heat radiated from a high temperature object (One  
which is not exposed to rain or water splash in case of indoor type)  
(3) A place which has a clean atmosphere (dust and corrosive gas not present)  
(4) A place with a minimum of vibration  
(5) A place where daily variation in temperature is minimum  
4.2 Selection of gas sampling location  
A place which satisfies the following conditions should be selected.  
(1) A typical place where the gases to be analyzed exist  
(2) Where the gases always flow without stagnation  
(3) A place easy of access for maintenance and inspection  
(4) Where the gases respond quickly to a change in the process operating conditions  
(5) Where variation in pressure, temperature, etc. is minimum  
2 –  
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4.3 Installation work  
For installation of the analyzer locker and the extractor, follow the piping instructions in Fig. 4-1 and the  
separately issued approval drawings (outline diagrams, sampling system diagram).  
(1) Countermeasures for cold climate  
(a) Freeze prevention of gas piping  
(b) Freeze prevention of drain pot  
(c) Freeze prevention of bypass and drain pipes  
(2) Countermeasurement for vibration  
When installing in a place where vibration is considerable, the locker should be floated on antivibration  
rubber pads.  
4.4 Connection of cables  
Caution  
Request an installation company or your dealer to carry out wiring.  
If wiring is incomplete, shock hazard or injury may be caused.  
Class D grounding construction is mandatory. Otherwise, shock hazard may be caused.  
<Caution for wiring company>  
For preventing shock hazard, fire and injury, be sure to observe the following.  
Before wiring, be sure to turn off the primary power supply. If this is neglected, you may receive and  
electric shock.  
For grounding, use a 600 V-IV wire having diameter of 2 mm2 or more and an adequate dielectric  
strength.  
Connect the power supply which meets the rating of product. Connection of other power supply may  
cause a fire.  
Select the diameter of input and output wires, which matches the rated current of gas analyzer.  
Be sure to use solderless terminals for connection to the input and output terminal block.  
Use the terminal block for branching the output wire.  
Be sure to fix the input and output wires onto the floor, wall surface, etc. and use a protective device for  
wires.  
The lead-in for AC power cables and outlet for signal wires are provided at the bottom of the analyzer or else  
at the specified place. Connect AC power cables and output signal wires according to the separately issued  
wiring diagrams.  
Note: Avoid connecting the analyzer power supply near devices such as high-frequency heating fur-  
nace or electric welder which greatly disturb the power waveform, and avoid sharing the same  
power lines with such devices. Class D grounding construction (100W ground resistance) is  
required.  
4.5 Connection of pipes (refer to piping instructions in Fig. 4-1 and separately issued approval  
drawings)  
(1) Connect gas pipe between the gas extractor and the analyzer inlet (sample gas inlet). Use a joint, etc.  
for ø10/ø8 Teflon pipe when connecting to ensure there will be no leakage.  
(2) Additionally tighten the joint section if necessary  
3 –  
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Fule  
(Note 1)  
300 or  
more  
Gas extractor  
ZBAK  
Note)  
Vertical  
300  
Horizontal  
installation  
(Note 2)  
Sampling  
pipe  
Leave 300mm space for inspection  
and exchange of filter.  
Gas outlet facing downward (or horizontal)  
Use termination kit TFC-7HPT-10JM (Note 6) or  
caulk with silicone bolding agent, etc. after  
insulation of heater wire (for indoor installation).  
Mating flange for  
installing extractor  
JIS 5K 65A FF  
*
Radius 300mm  
or more  
Heater power supply  
100V AC  
* Supporting wire  
Gradient of 15˚  
or more (Note 4)  
Teflon pipe φ10/φ8 or tube trace  
(heating pipe) SE-10C1-56-1-PVC-M  
or equivalent.  
Outer sheath for Teflon pipe ø10/ø8 is  
PVC and bundle outer sheath is ø33.  
* Support  
For pipe end processing, refer to Section 12.  
(Note 3)  
Peel off covering  
by about 2m.  
(φ10/φ8 teflon tube  
inside heating pipe)  
(Note 7)  
Power connection kit  
TFC-3HPT-10JM (Note 6)  
Gas  
conditioner  
Direct lead-in  
Filter  
*
Gas  
conditioner  
(in panel)  
(Note 7)  
Gas analyzer  
Sample tube  
(Note 5)  
60 × 120 square  
hole for wiring  
*Exhaust  
+ Drain  
Drain  
Drain  
Drain  
* Drain port (Note 8)  
Front-view diagram  
The part marked by the asterisk is not supplied.  
Fig. 4-1 Piping procedure  
Note 1) To prevent aspiration of leaked air  
Note 2) Install so that pipe end comes to nearly center of flue and is at right angle to the gas flow.  
Note 3) Peel off heating pipe by about 2m in order to air-cool measured gas.  
Note 4) Provide an inclination of 15° or more on the gas pipe so that drain will not accumulate in the event  
of power failure, etc.  
Note 5) Exhaust and drain share the same output. In the case of indoor installation, provide a drain pot  
and carry out drain separation, and exhaust air outside (pipe inner diameter should be ø8 or  
more).  
Note 6) Use this when utilizing a heating pipe. (Maker : Fujikin, Japan)  
Note 7) The gas pipe (ø10/ø8 teflon tube) should be inserted directly into the gas conditioner.  
Note 8) In outdoor application or in a cold district, protect the drain pot and pipes with a heat insulating  
material, etc. to prevent drain from freezing in winter.  
4 –  
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5. DESCRIPTION OF EACH PART  
Please refer to Chapter 14 specification attached at the end of the manual.  
6. PREPARATION FOR OPERATION  
6.1 Injection of clean water  
Inject clean water through the filter or air aspiration port until it overflows from the gas conditioner.  
6.2 Supply of external power  
Supply external power to the analyzer. And check the connections with output signal wire, etc. The exter-  
nal power supply should be.........  
100V±10% AC,  
50/60 Hz ±1%,  
with power consumption of 0.9kVA max. (excluding heating pipe).  
Check with reference to the separately issued approval diagrams.  
6.3 Check of sample piping, exhaust piping, etc.  
Check the connection of the sample piping and if necessary, provide exhaust piping + drain piping (Pipes  
with inner diameter of ø8 or more for both). When sample will be dispersed upward, then branch and water-  
seal the exhaust pipe for the purpose of drain separation. Be sure to disperse the exhaust into the atmo-  
sphere.  
Make checks with reference to the piping instructions in Fig. 4-1 and the separately issued gas analyzer  
diagram.  
5 –  
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6.4 Airtightness test  
(1) Piping inside panel  
Since airtightness is confirmed during tests before shipment, an Airtightness test during trial run is  
usually unnecessary. When a long time has passed after shipment, then carry out the following proce-  
dure.  
(a) Close the drain port.  
(b) Connect standard gas to the sample gas inlet.  
(c) Connect the transparent tube of the conditioner air suction port (see Fig. 10-1) vertically (in place  
of a manometer).  
(d) Flow standard gas gradually, and after reaching a pressure of about 1961Pa, close the needle valve  
of the pressure regulator.  
(e) Check the water level at the air suction port of the conditioner, and if the drop in the level in less  
than 147Pa/min, then the error due to insufficient airtightness is negligible.  
(f) If a leak is present when measuring a harmful gas, make a check by applying soapy water to the  
normal pressure section while aspirating outside air.  
(2) Piping outside panel  
Thoroughly check the tightened condition of pipe joints. If necessary, apply pressure from the extrac-  
tor outlet side and make a test as in the preceding item (1).  
(3) If the airtightness is insufficient, make a test on each section, find the faulty location and make it  
completely airtight. If the faulty location is before the aspirator, then air enters the gas pipe midway to  
cause a drop in the indication.  
6.5 Setting of temperature inside locker  
Turn on power supply to a space heater depending on the ambient temperature. Ventilation fan should  
always be turned ON.  
6.6 Warm-up time  
Turn ON the auto breaker.  
(1) Gas extractor  
Turn ON the power switch and warm up the extractor for at least 1 hour.  
(2) Heating pipe (option)  
Turn ON the power supply auto breaker of heating pipe and warm up the pipe for at least 1 hour.  
(3) Electronic gas cooler  
Turn ON the power switch and warm up for at least 10 minutes.  
(4) NO2/NO converter (option)  
Turn ON the switch, set the temperature regulator at 220°C, and warm up for about 30 minutes until  
indication of the temperature reaches 220±2°C. 200°C for a NO/CO (+ O2) analyzer  
(5) Analyzer  
Turn ON the power switch and carry out warm-up.  
Infrared gas analyzer: about 8 hours  
Zirconia O2 sensor: about 30 minuets  
6 –  
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7. INDICATION/OPERATION PANEL  
7.1 Name and description of each component of indication/operation panel  
3
4
5
6
Unit indication lamp  
Day indication  
Sub indication  
Range changeover switch  
2
1
Main indication  
Component indication  
SU TU TH SA  
MOWE FR  
Vol%  
ppm  
RANCE  
NOX  
SO2  
Vol%  
ppm  
RANCE  
RANCE  
Vol%  
O2  
HEAS  
CAL SET  
SET  
HOLD  
RANCE  
AUTO SAL  
CAL  
7
Function indicator lamp  
FUNC COMP  
ENT  
ZERO  
SPAN  
8
9
Function key  
Component selector key  
15 Calibration start key  
14 Span calibration key  
13 Zero calibration key  
12 ENT key  
10 Digit shift key  
11 Numeric input key  
(Three component of NOx, SO2 and O2 are indication in this figure.)  
Part Name  
Description  
q Component indication  
w Main indication  
Indicates kind of gas measured.  
Indicates measured concentration. Also indicates various set-points for alarm function, auto  
calibration function (option), etc.  
e Unit indication lamp  
r Day indication  
Indicates units of measured gas concentration.  
Indicates current day or day of starting by means of bar in auto calibration (option) setting mode.  
Indication SU  
MO  
TU  
WE  
TH  
FR  
SA  
Day Sun. Mon. Tue.  
Wed. Thu. Fri.  
Sat.  
t Sub indication  
Indicates measuring range, error code, various set points, etc.  
Used when changing the range. High range is set when pressing and low range is set when  
pressing  
y Range changeover key  
.
u Function indicator lamp  
MEAS:  
Relevant lamp lights up when following functions are set.  
Lights up in measuring status.  
CAL SET:  
Flashes in calibration concentration setting mode.  
ALM SET:  
Flashes in alarm setting mode.  
HOLD:  
Flashes in hold setting mode or lights steadily while hold function is activated.  
Flashes in remote range setting mode or light steadily while remote range function is activated.  
RMT RANGE:  
AUTO CAL:  
Flashes in auto calibration setting mode or lights steadily while auto calibration function is  
activated.  
i Function key  
Setting mode is changed at each press of this key (Refer to Section 5).  
Set component is changed for each setting mode.  
o Component selector key  
!
!
!
!
!
!
0
1
2
3
4
5
Digit shift key  
Shift is made from highest toward lowest digit at each press of this key.  
Selected digit is incremented at each press of this key.  
Numeric input key  
ENT key  
By pressing this key after setting, the set contents are memorized and becomes valid.  
Used for zero point calibration. (Lamp flashes in zero calibration mode.)  
Used for span calibration (Lamp flashes in span calibration mode.)  
Start key for manual calibration. Zero is calibrated by pressing ZERO and CAL keys.  
Span is calibrated by pressing SPAN and CAL keys. (CAL lamp lights steadily during calibra-  
tion).  
Zero calibration key  
Span calibration key  
Calibration start key  
7 –  
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7.2 Function and indication of indication/operation panel  
This panel consists of the following functions.  
Key  
Function  
Main indication  
Measuring value  
Sub indication Function indication lamp  
FUNC  
Measuring mode  
Range  
MEAS lamp lights  
Setting mode  
FUNC  
FUNC  
FUNC  
FUNC  
FUNC  
FUNC  
FUNC  
FUNC  
FUNC  
FUNC  
FUNC  
Calib.conc.setting  
Calb.conc.  
Range  
CAL SET lamp lights  
ALM SET lamp flickers*  
HOLD lamp flicker  
Alarm setting (option)  
Hold setting  
Alarm value  
ON or OFF  
ON or OFF  
Day  
Remote range setting (option)  
Current time setting  
RMT RANGE lamp flickers*  
Auto CAL lamp flickers  
AUTO CAL lamp flickers  
AUTO CAL lamp flickers  
AUTO CAL lamp flickers*  
AUTO CAL lamp flickers*  
AUTO CAL lamp flickers  
*
Hr.min.  
Auto clib.start time setting  
Auto calib.cycle setting  
Calib. gas flow time setting  
Calib. gas flow time setting  
Auto calib.changeover  
Key lock changeover  
HR.min.  
Day  
Time  
Time  
Mode No.  
ON or OFF  
ON or OFF  
ZERO  
ZERO  
Zero calibration  
Span calibration  
Measured value  
Measured value  
Range  
Range  
Zero key indication flickers  
Span key indication flickers  
When the setting mode is assumed, the analog output signal is held at the value just before entering this mode.  
When optional functions are not provided, the contents of these functions are not indicated.  
* Refer to the instruction manual of the infrared gas analyzer for the items marked by the asterisks.  
8 –  
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7.3 General operation of indication/operation panel  
The measuring mode is assumed when  
power is turned ON. The gas concentra-  
tion appears on the main indication, while  
the range being used appears on the sub in-  
dication.  
NO  
Gas concentration  
indication  
Range  
indication  
Advice on Operation  
Hige rang is selected  
when key is pressed  
LWhen selecting the range  
In the setting status, as shown in the figure  
at the right, the high range is selected when  
key is pressed, while the low range is  
selected when key is pressed.  
Low rang is selected  
when  
key is pressed  
LWhen selecting the gas component  
In the setting status, as shown in the figure  
at the right, the gas component can be set  
by pressing COMP key.  
1st component  
2rd component  
3rd component  
Example: When COMP key is pressed  
while the 1st component is flash-  
ing, the flashing moves to the  
2nd component (figure at right).  
The setting for the 2nd compo-  
nent is now changeable.  
COMP  
ENT ZERO SPAN CAL  
* The 1 component type analyzer is not pro-  
vided with COMP key.  
Pressing changes the settable gas component.  
ZERO SPAN  
LFor releasing zero or span  
If a mistake has been made in zero or span  
calibration, then perform a reset in the fol-  
lowing way.  
Pressed wrongly.  
ZERO SPAN  
The figure at the right shows an example.  
If SPAN key has been pressed mistakenly  
instead of ZERO key, then press SPAN  
key again. Calibration is released.  
The lamp blinks.  
ZERO SPAN  
Press again to extinguish the lamp.  
Thus reset. Press the  
key afresh.  
ZERO  
If ZERO key has been pressed mistak-  
enly instead of SPAN key, the press  
ZERO key again.  
Calibration is released.  
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8. CALIBRATION  
Danger  
When handling standard gas such as calibration gas, read the instruction manual for the standard gas for  
correct handling. Special care should be taken when handling hazardous gas such as CO gas and the like  
to prevent poisoning.  
8.1 Kinds of standard gas  
8.1.1 When not using zirconia O2 sensor  
(1) Zero gas: N2 or atmospheric air/instrument air depending on specification (when without verifi-  
cation stipulated in the laws for measurement and weighing)  
(2) Span gas: Gas of 90% or more full scale for each component, remainder is N2 (span gas for low  
range will be delivered unless otherwise specified)  
8.1.2 When using zirconia O2 sensor  
(1) Zero gas: Air (Span gas of the O2 analyzer in the laws for measurement and weighing).  
(2) Span gas: 1 to 2% O2, remainder is N2. (Zero gas of the O2 analyzer in the laws for measurement  
and weighing).  
Gas of 90% or more full scale for other than zirconia O2 sensor, remainder is N2.  
Note: For separately calibrating the low and high ranges of the zirconia O2 sensor, supply 9 to  
10% O2 and the remainder N2 for the low range (10%) and use air for the high range  
(25%).  
8.2 Preparation of standard gas  
The standard gas to be used for calibration is delivered in a separate package from the locker.  
Check the kind of standard gas to be used according to the sampling system diagram, and set it at the  
prescribed location.  
Before starting calibration, attach a pressure regulator to the standard gas.  
8.2.1 How to mount pressure regulator for standard gas cylinder  
(1) Before mounting a pressure regulator to the gas cylinder, clean the gas cylinder adapter. Entry of  
dust into the pressure regulator may result in gas leaks.  
(2) If packing is not inserted in the mounting nut for the cylinder or it is damaged, replace it with  
supplied spare one.  
(3) Use a spanner of a proper size, fasten the cylinder mounting nut to the gas cylinder. Mount  
supplied joint to the outlet according to Item Sampling system block diagram.  
(4) Loosen the pressure controls and then tighten the outlet controls.  
(5) Open a valve of the gas cylinder, and the pressure gauge on the high pressure side indicates a  
pressure of the gas cylinder by flowing gas into the pressure regulator.  
(6) Turn the pressure controls clockwise to increase the secondary pressure; adjust the pressure con-  
trols so that a pressure gauge on the low pressure side reads 30 kPa.  
(7) Open the outlet controls to release gas.  
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Adapter  
Pressure gauge on  
high pressure side  
Pressure gauge on  
low pressure side  
Pressure controls  
Packing  
Cylinder mounting nut  
Pressure regulator  
Cylinder  
R1/4 joint  
Output handle  
Fig. 8-1 Pressure regulation for standard gas cylinder  
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8.3 Calibration concentration setting (except zirconia O2 sensor)  
Set a span value for the calibration concentration setting. (Zero point calibration concentration is fixed at  
zero.)  
Set the calibration gas concentration (span value).  
NO  
When FUNC key is pressed in the measuring sta-  
tus, the previously set span value will appear on  
the main indication.  
FUNC  
The CAL SET LED of the function indicating  
lamps will flicker.  
NO  
By pressing the  
key, the highest digit of the  
main indication for the 1st component will flicker,  
and the span value can not be set.  
CAL SET  
Select a range with the  
keys.  
NO  
NO  
NO  
After selecting the range, set a span value in this  
status.  
The numeric value will be incremented by press-  
ing  
key.  
The digit to be set can be selected by pressing  
key.  
ENT  
For selecting the 2nd and subsequent compo-  
nents and the range, press the  
key and  
while the main indication for the 1st compo-  
nent is flickering, press the COMP key and  
then the main indication for the component to  
be set will flicker. Now press the  
select the range to be set.  
keys to  
When the span value has been set, press the ENT  
key. Setting operation is completed.  
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[When adjusting for each range]  
(Simultaneous calibration of H and L ranges has been factory-set).  
Perform setting in the following way.  
NO  
By pressing CAL key while the highest digit of the  
main indication for the 1st component is flickering,  
CAL  
then ‘  
will appear on the main indication and  
‘ ’ will appear on the sub indication.  
NO  
NO  
NO  
Press  
key and will change to  
.
= Meaning of set values =  
: The calibration is valid only for the selected  
range, and zero and span calibration can  
be made independently for each range.  
By conducting zero and span calibration  
for one range, the calibration will be done  
automatically for the other ranges as well.  
ENT  
:
When the selection has been finished, press the ENT  
key. Setting operation is completed.  
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8.4 Calibration concentration setting (zirconia O2 sensor)  
A zirconia O2 sensor sets the zero (air) point (span point stipulated in the laws for measurement and  
weighing) of the O2 analyzer. For the density of calibration gas to be used, refer to 8.2 Preparation of  
standard gas.  
LSetting of calibration concentration for zero (air)  
point (zero stipulated in the laws for measurement  
and weighing)  
By pressing the FUNC key in the measuring status,  
O2  
the calibration concentration previously set for the zero  
(air) point will appear on the main indication.  
FUNC  
The CAL SET LED of the function indicating lamps  
will flicker.  
O2  
By pressing the  
key, the higher digit of the main  
indication of the O2 analyzer will flicker and zero point  
setting is enabled.  
CAL SET  
Press the  
keys to select a range.  
O2  
O2  
O2  
The numeric value will be incremented by pressing  
key. The digit to be set is selected by pressing the  
key.  
Setting ranges are 20.2 to 21.9 Vol. % for high  
range and 7.0 to 21.9 Vol. % for law range.  
ENT  
Set the air concentration for both high and low  
range.Note)  
Press the ENT key after setting the zero point. Set-  
ting operation is completed.  
Note: When using air for the high range and 9 to 10 Vol. % O2/N2 for the low range, set the density  
for each range.  
When viewing from the zirconia O2 sensor side, the air point corresponds to the zero point.  
Therefore, calibration should begin with the air point.  
Also, since the air point and low concentration point can be calibrated by the zero calibra-  
tion key and span calibration key, respectively, the air point and low concentration point  
are regarded as the zero and span in this manual.  
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LSetting of span calibration concentration (zero point  
stipulated in the laws for measurement and weigh-  
ing)  
Setting of each component  
Press the CAL key in the status where the digit of the  
O2 analyzer main indication is flickering via the zero  
(air) point calibration concentration setting.  
O2  
CAL  
The previously set span value will now appear on the  
main indication.  
NO  
The CAL SET LEDof the function indicating lamps  
COMP  
will flicker.  
O2  
O2  
O2  
Then, press the COMP key and the highest digit of  
the 02 analyzer main indication will flicker and the  
span value is now settable.  
Press the  
keys to select a range.  
When the range has been selected, set a span value in  
this status.  
ENT  
The numeric value will be incremented by pressing  
the  
key.  
Press the  
lected.  
key and the digit to be set can be se-  
Press the ENT key after setting the span value. Set-  
ting operation is completed.  
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8.5 Zero calibration (air point calibration in case of zirconia O2 sensor)  
This is used for adjusting the zero point.  
Flow the zero gas (0.3N/min.) by adjusting the needle  
valve of pressure regulator and wait until the indica-  
tion stabilizes.  
When the Zirconia O2 sensor is used, use air.Note)  
NO  
NO  
ZERO  
When the indication has stabilized, select the measur-  
ing range to be calibrated by using the  
keys.  
Flickers  
When using a multi-component analyzer, all the  
components undergo zero calibration simulta-  
neously at the selected range.  
ENT ZERO SPAN CAL  
CAL  
ZERO  
Press the ZERO key, and  
flicker.  
key lamp will  
NO  
Lights  
Next press the CAL key and conduct zero calibra-  
tion.  
ENT ZERO SPAN CAL  
CAL  
The  
key lamp lights steadily during calibra-  
ENT ZERO SPAN CAL  
tion.  
( Lamp is turned off after calibration )  
Since the measuring status is resumed after the cali-  
bration, carry out the calibration for other ranges if  
necessary.  
Note: When using different gases for the low and high ranges, apply 9 to 10 Vol. % O2/N2 which has  
been set for the low range.  
When the function for automatic calibration is provided, the solenoid valve turns on and cali-  
bration gas flows upon pressing the ZERO key.  
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8.6 Span calibration (low concentration point calibration in case of zirconia O2 sensor)  
Carry out span calibration by flowing calibration gas at  
the concentration set as a span value.  
NO  
Flow the calibration gas (0.3 N/min.) by adjusting the  
needle valve of pressure regulator. Wait until the indica-  
tion stabilizes, and then conduct span calibration.  
SPAN  
SPAN  
Press the SPAN key and the  
key lamp flickers.  
NO  
Flickers  
In the case of a multi-component analyzer, the main  
indication will flicker for the components which  
can be calibrated.  
ENT ZERO SPAN CAL  
(
)
COMP  
Press the COMP key and the settable gas compo-  
nent will change.  
When the gas component has been determined,  
NO  
press the  
keys and select a range.  
Note: The lamp will not flicker in the case of a  
single-component analyzer.  
Flickers  
ENT ZERO SPAN CAL  
(In case of a multi component analyzer)  
Next press the CAL key and conduct span calibration.  
CAL  
CAL  
The  
key lamp lights steadily during calibration.  
NO  
Since the measuring status is resumed after calibration,  
continue the calibration for each component and each  
range.  
lights  
ENT ZERO SPAN CAL  
ENT ZERO SPAN CAL  
( Lamp is turned off after calibration )  
Note: On the low range of zirconia type O2 sensor, when zero gas is calibrated with 9 to 10 Vol. % O2,  
the zero and span calibrations interfere with each other. So, each calibration should be re-  
peated a few times.  
When the function for automatic calibration is provided, the solenoid valve turns on and the  
span gas for the selected component flows upon pressing the SPAN key.  
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8.7 Auto calibration  
In this analyzer, the signals form the input/output terminals on the upper can be used for driving an external  
solenoid valve and introducing standard gas, whereby zero point and span can be calibrated automatically.  
The auto calibration is done according to 8.7.1 Current time setting, 8.7.2 Auto calibration start time setting,  
8.7.3 Auto calibration cycle setting, 8.7.4 Auto calibration ON/OFF setting and 8.7.5 Output Hold setting at  
Calibration.  
Cautions on operation  
1. When the auto calibration start time is reached during key operation, the auto calibration is given  
priority and is started. All key operation will be invalid until the auto calibration is finished.  
2. To forcibly interrupt the auto calibration in progress, press both the ENT and CAL keys simulta-  
neously. After the forcible interrupt, the measuring mode is resumed and all the keys are operable.  
Although the current auto calibration will be passed over, it will be started from the initially set  
cycle from the next time onward.  
Example: When auto calibration is set for 3 hour intervals starting from 8:00 a.m.  
: Under auto calibration  
8 : 00  
11 : 00  
14 : 00  
17 : 00  
8 : 00  
11 : 00  
14 : 00  
17 : 00  
Forcible interruption  
3. Key operation is possible while calibration is not under way with the auto calibration function set.  
Therefore all settings (of span, hold, remote range, time, etc.) including manual calibration can be  
made. But note that if the wrong time is set on the clock, the auto calibration will not be started at  
the correct time.  
4. Auto calibration is able to start by applying remote start input signal, 5V DC longer than 100msec,  
to remote start input terminals. In this case, auto calibration will start independent to its ON/OFF  
setting. (Calibration starts at the trailing edged of signal.)  
5. When measuring 4 components, or NOx, SO2, CO and O2 (with 2 infrared gas analyzers), the auto-  
matic calibration cycle should be set on the CO/O2 analyzer side and the automatic calibration of  
NOx/SO2 analyzer should be turned OFF. After the automatic calibration of CO/O2 analyzer, the  
automatic calibration of NOx/SO2 analyzer will be started.  
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Example of auto calibration time chart for 4-component measurement  
Auto calibration start time  
Under  
Under auto calibration  
measurement  
Zero  
gas  
Span  
gas 1  
Zero  
gas  
Span  
gas 1  
Span  
gas 3  
Substi-  
tution  
Span  
gas 2  
Span  
gas 3  
SO2  
CO  
O
2
NO  
O
2
Gas flow time  
Auto calibration  
gas flow time  
T
T
T
T
T
T
T
T
T: settable from 100 to 599 sec. (Note)  
Auto calibration cycle  
Gases introduced:  
Sample gas  
Zero gas  
Span gas 1  
CO  
Span gas 1  
NO  
Span gas 2  
SO2  
Span gas 3  
O2  
Indicator lamps  
AUTO CAL.  
Flickers  
ZERO  
SPAN  
CAL  
Flickers  
Lights  
HOLD  
(at HOLD ON)  
Auto calibration abnormality:  
If an abnormality occurs during auto calibration, a contact signal for auto calibration abnormality will be  
output from the input/output terminals on the upper of the analyzer. The gas which incurred the abnormality  
will not be calibrated, and instead the next component will be calibrated.  
Note: Usually, T is set at 360 sec. for measurement including SO2, and at 180 sec. for other measurements.  
For change of setting, refer to the separate instruction manual of infrared gas analyzer.  
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8.7.1 Current time setting  
Set the current time and day of the week.  
FUNC  
Press the FUNC key in the measuring status.  
The AUTO CAL LED of the function indicating lamps  
will flicker.  
SU TU TH SA  
MO WE FR  
NO  
The main indication shows the hour and minute via a  
24-hour indication and the decimal point flickers.  
A’–’ bar lights up at the relevant weekday on the sub  
indication.  
AUTO CAL  
Flickers  
(
)
SU TU TH SA  
NO  
NO  
NO  
Indication SU MO TU WE TH FR SA  
MO WE FR  
Day  
Sun. Mon. Tue. Wed. Thu. Fri. Sat.  
key and the time is now settable.  
(
)
Press the  
SU TU TH SA  
The highest two digits of the main indication will flicker.  
MO WE FR  
ENT  
The numeric value is incremented by pressing the ‘  
.  
SU TU TH SA  
MO WE FR  
Press the  
key and the digit can be selected.  
After the time setting, press  
on the sub indication.  
key and the day is settable  
The bar indication will flicker.  
Press the  
key and the bar will shift.  
Press the ENT key when the time and day setting is fin-  
ished. The data are saved.  
Time starts from the point where ENT key is  
pressed.  
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8.7.2 Auto calibration start time setting  
When FUNC key is pressed at the current time indica-  
tion, the auto calibration start time and day will appear on  
the main and sub indications.  
SU TU TH SA  
MO WE FR  
NO  
Lights  
The AUTO CALLED of the function indicating lamps  
will flicker. In the case of start time, the decimal point on  
the main indication will light steadily.  
FUNC  
SU TU TH SA  
MO WE FR  
NO  
Press the  
key and the auto calibration start time is  
AUTO CAL  
settable, so set a start time on the main indication.  
(
)
The numeric value is incremented by pressing the  
key.  
SU TU TH SA  
NO  
NO  
NO  
MO WE FR  
Press the  
key and the digit can be selected.  
(
)
SU TU TH SA  
After setting the calibration start time, press the  
key  
and the calibration start day can be set on the sub indica-  
tion.  
MO WE FR  
ENT  
The bar indication will flicker.  
SU TU TH SA  
MO WE FR  
Press the  
key and the bar will shift.  
The auto calibration start time is settable up to one  
week ahead.  
When the auto calibration start time and day have been  
set, press the ENT key. The data are saved.  
When the auto calibration at the set time is fin-  
ished, the next auto calibration start time will be  
set automatically.  
To confirm the next auto calibration start time, then  
carry out this operation and check the indication.  
Note: When the auto calibration start time has been set, then set the auto calibration cycle.  
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8.7.3 Auto calibration cycle setting  
The calibration cycle is settable in either dayss or hours.  
Press the FUNC key at the calibration start time indica-  
NO  
NO  
tion and ‘  
will appear.  
FUNC  
The AUTO CAL LED of the function indicating lamps  
will flicker.  
Press the  
The highest digit on the sub indication will flicker. Select  
either daysor hoursby pressing the key.  
key and the auto calibration cycle is settable.  
AUTO CAL  
(
)
‘ ’ appears on the sub indication when selecting  
daysand ‘ ’ appears when selecting hours.  
NO  
NO  
NO  
(
)
Press the  
key and the calibration cycle and be set in  
the lower digits of the sub indication.  
The numeric value is incremented by pressing the  
key.  
ENT  
Press the  
key and the digit can be selected.  
Day is settable in a range of 1 to 7 days. Hour is  
settable in a range of 1 to 99 hours.  
Note  
If 0 0(hours) is set, it will be automatically set  
to 1(hours).  
Press the ENT key when the calibration cycle has been  
set. The data are saved.  
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8.7.4 Auto calibration ON/OFF setting  
Select whether or not to carry out auto calibration.  
when calibration will not be made.Note)  
NO  
NO  
Set to ‘  
Press the FUNC key at the calibration gas flow mode  
indication and ‘ ’ will be appear.  
FUNC  
The AUTO CAL LED of the function indicating lamps  
will flicker.  
AUTO CAL  
Press the  
be set.  
key and auto calibration ON or OFF can  
Select either ‘  
or ‘  
on the sub indication by  
NO  
NO  
NO  
pressing the  
key.  
When the auto calibration ON/OFF setting is finished,  
press the ENT key. Setting operation is completed.  
ENT  
Note: In case of 4-component (NOx, SO2, CO and O2) analyzer, be sure to turn OFF the automatic  
calibration of NOx/SO2 analyzer.  
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8.7.5 Setting of output hold at calibration  
This is used when calibrating for holding the output sig-  
nal at the value just be before entering calibration. (The  
indication is not held.)  
The hold function is settable for each component.  
FUNC  
Press the FUNC key in the measuring status and  
NO  
will be indicated.  
HOLD  
The HOLD LED of the function indicating lamps will  
flicker.  
Press the  
key and the hold function will be settable.  
NO  
NO  
NO  
The sub indication will flicker.  
Select hold ‘  
or ‘  
by pressing the  
key.  
Press the ENT key after setting the hold function. Set-  
ting operation is completed.  
ENT  
Setting is valid for all the components.  
At hold ON, the HOLD of the function indicating lamps  
will light steadily while the hold function is activated.  
At hold OFF, these lamps will go off.  
In case of automatic calibration, output is held while the  
automatic calibration lamp is lit.  
In case of manual calibration, output is held for about half  
an hour after completion of calibration.  
For canceling the output hold forcibly, turn off the hold  
setting once.  
Note 1: When measuring 4 components, or NOx, SO2, CO and O2 (with 2 infrared gas analyzers),  
output is held by using the external hold function at the time of automatic calibration.  
Note 2: In the setting mode, output is held indifferently to the ON/OFF status of hold setting.  
Note 3: In case the analyzer is equipped with a maintenance switch, output is held while the switch  
is turned on.  
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9. OPERATION  
Danger  
If you notice malodor or abnormal sound, stop the instrument immediately. If this is neglected, fire may  
occur.  
Caution  
When the analyzer is to be operated after it has been left unused for a long time, the operating procedure  
is different from the normal stop/start procedure. It should be handled according to the procedure shown  
in the instruction manual to ensure its proper performance and to prevent trouble or injury.  
Do not operate the analyzer for a long time with its door left open to avoid entry of dust into the analyzer.  
Dust deposits will result in damage to the analyzer.  
Prohibition  
Do not insert a rod or your finger into the fan (electronic cooler at ceiling), otherwise injury may be  
caused by the rotating blades.  
Do not touch metal, finger, etc. to the input and output terminal block of analyzer. Otherwise, shock  
hazard or injury may be caused.  
Smoking and use of fire/flame is prohibited in the vicinity of the gas analyzer. Otherwise, a fire may  
occur.  
A water-filled container such as a bucket should not be placed on the roof of the gas analyzer having  
indoor specifications. If such a container turns over, spilled water may cause shock hazard or burning  
inside the analyzer.  
9.1 Operating procedure  
(1) Check if all the preparation for operation have been completed.  
(2) Press the range selector switch on the indication/operation panel to select a range to be used.  
(3) Press the function key FUNCon the indication/operation panel to light up the MEASfunction  
indicator lamp.  
(4) Turn on the aspirator power supply and confirm that the ball of flow meter is at 0.4N/min.  
Prescribed flow rate may be 0.5N/min. So it should be checked in the piping system diagram sepa-  
rately presented.  
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10. MAINTENANCE  
Danger  
• When handling standard gas such as calibration gas, read the instruction manual for the standard gas for  
correct handling. Special care should be taken when handling hazardous gas such as CO gas and the like  
to prevent poisoning.  
• During maintenance or inspection, be sure to turn ON the ventilation fan in the analyzer to prevent  
poisoning due to gas leakage.  
• When the gas filter of the analyzer is to be replaced or the washing unit needs maintenance, be sure to  
close the calibration gas valve. Especially, if the calibration gas valve is located at the sample gas inlet,  
the replacing or washing shall be done after closing the calibration gas valve to prevent poisoning or  
other trouble.  
Caution  
• The gas converter is heated to about 220°C. When the catalytic agent needs to be replaced, turn OFF the  
power for the converter and use heat-proof gloves about 30 minutes later.  
• When the fuse is blown off, check the cause of it and replace it with the same type of fuse having the  
same capacity to prevent electric shocks or other trouble.  
• When the analyzer is provided with a power leak relay, press the test button to confirm proper operation  
before making maintenance or inspection to prevent electric shocks.  
• Be sure to lock the door. Do not allow unauthorized persons to use the door key. Do not touch the door  
carelessly to prevent electric shocks and other trouble.  
The following items must be observed to prevent electric shocks or injury and to ensure safety.  
• Take off metallic objects such as wrist watch before starting the work.  
• Do not touch the device with wet hands.  
10.1 Routine maintenance and inspection  
Maintenance/inspection item  
Procedure  
Monitoring of sample flow rate  
Monitoring of conditioner bubbling quantity  
Prescribed flow rate: The flow rate is normal when the ball is at  
0.4N/min. and there is slight bubbling at the bottom of conditioner.  
Adjust the needle valve so that a flow rate of 0.4N/min. is available.  
If the prescribed flow rate is unobtainable even with the needle valve  
fully open though there is slight bubbling, then the capillary (sample  
line) should be checked for clogging. In case there is no bubbling, the  
aspirator, conditioner, electronic cooler and pipe should be checked for  
clogging. And if water decreases in the conditioner because of heavy  
bubbling, the capillary of bypass line should be checked for clogging.  
(Note)  
Good if H2 level shown in Fig. 10-1 is longer than 100mm.  
If air is aspirated through the air aspiration tube, then the pressure loss at  
the stage before the conditioner filter has become large. Check the gas  
extractor filter (see (1) in 10.5) and gas pipes for clogging.  
Conditioner  
Air aspiration tube level  
– 26 –  
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Maintenance/inspection item  
Procedure  
Contamination of membrane filter  
Replace the filter paper if it has blackened (see (3) in 10.5).  
If contamination occurs rapidly, then check the pre-stage filters of the  
gas extractor ((1) in 10.5), conditioner filter ((2) in 10.5), etc.  
Electronic gas cooler  
Check the fan rotation.  
Temperature controller for NO2/NO converter Check that the controlled temperature is approx. 220°C (200°C in case  
of NO/CO analyzer).  
Note) Bubbling will be eliminated when a pressure control valve is equipped.  
Prescribed flow rate value should be checked in the piping system diagram separately presented.  
Conditioner filter  
O-ring (G65)  
Fastening nut  
Wing bolt  
Sample gas  
To analyzer  
Water  
injection  
Aspirator  
Upper chamber  
Electronic  
gas cooler  
Air  
aspiration  
pipe  
H2  
Capillary  
or  
Pressure  
control valve  
Bypass  
Capillary  
H1  
H1: Sample negative pressure  
Exhaust after analysis  
H2: Good when longer than 100mm.  
Be careful when within 50 to 100mm.  
Check extractor filter piping when  
shorter than 50mm.  
Lower chamber  
Drain and exhaust  
Slight bubbling  
(Bubbling is eliminated when  
the unit is provided with  
pressure control valve.)  
Fig. 10-1 Conditioner  
27 –  
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10.2 Periodic maintenance and inspection  
Maintenance/inspection item  
Analyzer calibration  
Referential frequency  
Weekly  
Procedure  
Refer to section 8.5 to 8.6.  
Check of standard gas filled  
pressure  
It takes at least 1.5 months to deliver the standard gas. So  
the gas should be ordered 2 or 3 months in advance.  
Water level in upper chamber of  
conditioner  
Monthly  
Every two months  
Biannually  
Supply water if level is below overflow port.  
Replacement of membrane filter  
paper  
Replace with new filter paper (stop the aspirator when  
exchanging). See 10.5 (3).  
Inspection and replacement of  
conditioner filter, O-ring  
Replace these parts if flow rate doesnt increase because of  
adherence of dust. See 10.5 (2).  
Capillary  
Replace if clogged.  
Check of valve and diaphagm of  
aspirator (pump)  
Check and clean diaphragm. Use valve by turning it to 90°  
rightward (replace valve when it is turned once). See 10.5  
(4).  
Leak test of pressure regulator  
Replacement of standard gas  
Apply soapy water or the like and check for bubbles. Either  
retighten or replace packings if necessary.  
NO, SO2, CO/N2 of less than 250 ppm. See 10.4.  
Replacement of gas extractor filter  
element, O-rings  
Yearly  
O-ring requires replacement. Filter element may be reusable  
after cleaning. See 10.5 (1).  
Catalyst of NO2/NO converter  
Replacement (when NO2 gas concentration is 10 ppm or  
less)  
Note: Replace once every 8 months when NO gas con-  
centration is measured in the setting range of 0 to  
200ppm or more at 0.5L/min.  
Replacement of standard gas  
Aspirator  
See 10.4.  
Replacement of diaphragm  
Clean pipes or replace if necessary.  
Contamination, leak test of piping  
Exchange of water in conditioner  
Overhaul  
10.3 Other maintenance and inspection  
(1) Space heater and ventilating fan  
If the ambient temperature drops below 5°C during winter or the like, then turn ON the space heater.  
The ventilating fan should always be left ON.  
(2) Blowback of gas extractor (option)  
Turn off the aspirator and close the measured gas line before conducting a blowback. Frequent blowback  
will cause the temperature of the gas sampler to drop and result in corrosion, so it should be kept to a  
minimum.  
28 –  
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10.4 Concentration guarantee term of standard gas cylinder (for NOx, SO2, CO and O2 analyzer)  
Kind of gas  
NO/N2  
NO/N2  
SO2/N2  
SO2/N2  
CO/N2  
CO/N2  
O2/N2  
Concentration range  
0.4ppm or more, and less than 250ppm  
250ppm or more, and less than 5%  
0.4ppm or more, and less than 250ppm  
250ppm or more, and less than 1 %  
2.4ppm or more, and less than 100ppm  
100ppm or more, and less than 15%  
0.9% or more, and less than 25%  
Guarantee term  
6 months  
1 year  
6 months  
1 year  
6 months  
1 year  
1 year  
N2  
*None  
Air  
*None  
* Schedule the use for about one year under proper control.  
Note: It is empirically known that standard gas concentration remains within the adequate accuracy  
for 6 months or 1 year. However, gas makers guarantee term is as listed in the above table.  
Therefore, replacement is required within the guarantee term when importance need be placed  
on traceability.  
10.5 Maintenance of sampling device  
(1) Replacement of filter element of gas extractor (extractor type : ZBAK1)  
(a) Turn off power supply to the extractor  
(b) Turn off the pump of gas analyzer  
(c) After making sure the temperature of extractor has dropped adequately, detach the rainproof cover  
(remove the wing bolt on the flange side).  
(d) Remove the locking wing bolt and pull out the internal parts while gripping the handle for filter ex-  
change.  
Although you may feel slight stiffness in pulling out the handle for filter exchange, it should be pulled  
out gradually while turning it.  
(e) Remove the metallic mesh filter from the seal fixture.  
(f) After mounting a new element, reverse the above procedure.  
Locking wing bolt  
Seal fixture  
Filter case  
Handle for filter exchange  
O-ring  
(JIS P48A Viton)  
Metallic mesh filter  
Fig 10-2 Gas extractor (type ZBAK1)  
29 –  
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(2) Replacement of mist filter element (See Fig. 10-1.)  
(a) Loosen the butterfly bolt, and pull the head up and out of the container.  
(b) Then loosen the retaining nut and remove the contaminated filter element.  
(c) Replace with a new conditionor filter and O-ring, and reassemble by reversing the above steps.  
(3) Replacement of membrane filter element  
(a) Turn off the power to the gas aspirator (pump).  
(b) Turn the lid of the membrane filter counterclockwise and remove it.  
(c) After removing the lid, detach the inner O-ring and replace the filter element.  
(d) Wipe dust out of the case by using a clean cloth. Be careful not to let dust enter the gas outlet side.  
(e) After replacing the filter, reassemble by reversing the above steps.  
(f) Attach the flouro pour filter closely to the filter supporting bracket.  
(g) Apply vacuum grease about once every 6 months to the O-ring.  
Filter element  
Lid  
Inner O-ring  
Outer O-ring  
Case  
Supporting bracket (used with fluoro-pour filter)  
Fig. 10-3 Membrane filter  
30 –  
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(4) Replacement of the valve and the diaphragm of diaphragm type aspirator  
Replace the seat valve (turn 90° in six months and replace annually) and the diaphragm (replace annually)  
according to the following procedure.  
(a) Turn off the power supply of the aspirator and  
remove the inlet and outlet piping connected to  
the aspirator.  
(b) Remove the four hexagon socket head cap  
screws. Then cap A and cap B are separated  
and the valve can be removed.  
Hex. socket head  
cap screw  
(c) Turn the diaphragm counterclockwise with your  
hand and remove it.  
Cap A  
(d) Place a new diaphragm to the position and mount  
it by turning it clockwise until it stops.  
Note) When mounting, check that the dia-  
phragm is securely engaged in the  
screw section of the arm slot. Other-  
wise malfunction may result.  
Rc1/8  
Seat valve  
Cap B  
(e) Place the valve on cap B and turn it 90. Check  
that the notches of cap A and cap B are aligned,  
and then tighten the four hexagon socket head  
cap screws.  
Diaphragm  
Note) Since complex valve seat is adopted, re-  
move the pin on the underside of the  
valve from the hole to which the pin has  
been inserted and reinsert it to the  
other hole.  
Arm lot  
(f) Turn on the power of the aspirator in the inter-  
face module. Check that it does not generate  
abnormal sound. Check also with your hand that  
the valve is normally operated, that is, air is as-  
pirated from the IN side and discharged from  
the OUT side. If any abnormality is observed,  
repeat the procedure from the beginning.  
(g) After checking that the aspirator is normally op-  
erated, turn off the power of the aspirator in the  
interface module, and return the piping to the  
original position.  
Fig. 10-4 Exploded view of diaphragm type aspirator  
Note) Do not apply force abruptly to Rc1/8  
screw part when returning the piping  
to the original position.  
31 –  
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(5) Check and maintenance of electronic gas cooler  
(a) Fan motor  
This motor should be replaced periodically every 20,000 hours (about 2 years in case of continuous  
operation ) as a standard though this varies with operating condition. However, if no abnormality  
cannot be found at the time of a periodic replacement, the motor is further usable continuously.  
(b) Gas passage cleaning procedure  
When bubbling has come to diminish significantly, it can be thought that the passage has come to be  
clogged by dust, etc.  
In this case, the gas passage needs be cleaned in the procedure given below.  
(i) When looking at the inside of INLET joint, area B of the  
INLET joint  
spiral guide can be seen. In the area B, a lateral hole of  
C
1.5mm dia. is bored. So, insert the top of the furnished  
OUTLET  
INLET  
spiral pull-out device into the hole as shown below and  
extract the spiral guide.  
(ii) Clean the gas passage and spiral guide. For detergent,  
use a one having a chemical composition which will not  
affect hard glass, hard PVC, polyethylene and fluoro-  
rubber. After washing, rinse adequately with water and  
dry the inside well by blowing compressed air.  
B
Spiral pull-out  
device  
Spiral guide  
Heat exchanger  
(iii) When inserting the spiral guide to the original position,  
it should be pressed lightly until area A of the spiral guide  
comes in contact with the bottom. As a standard, area B  
of the spiral guide should be located with a distance L of  
about 15 to 20mm from the top face C of INLET joint.  
Note that attention should be paid since piping is stepped.  
A
Note) For sampling with the pressure control valve, clean  
the gas passage using the above procedure when  
the sample flow begins to be extremely reduced.  
DRAIN  
Fig. 10-5 Structure of electronic dehumidifier  
32 –  
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(6) Replacement of NO2/NO converter catalyst  
(a) Turn off power supply to the converter.  
(b) After half an hour, remove q w e, and extract r  
upward and downward, respectively. Pay attention  
not to suffer a burn. In addition, carefully handle the  
ceramic pipe for preventing breakage. When remov-  
ing r , e will fall simultaneously. So prepare a  
catalyst receiver.  
q Connection  
rubber  
Ring  
w
e Filter  
r Catalyst  
Filter  
e
t
Fastener  
(c) Wind glass wool on the tip of r and insert it from  
the bottom together with q. Inject one pack of new  
catalyst from the top. Set w e on the top side. (This  
step is unnecessary when a membrane filter is pro-  
vided at the later stage.)  
Ceramic  
pipe  
y
q Connection  
(d) Connect the pipe, set the temperature controller at  
220°C (200°C for NO/CO analyzer), and turn on  
power supply.  
rubber  
Fig. 10-6 Structure of NO2 /NO converter  
(7) Setting of temperature controller for NO2/NO converter (PXZ4)  
(a) When pressing the PV/SV key, display changes over between PV and SV. (Usually, PV (Process  
Variable) display is set).  
(b) Under SV (Set Value) display, set 220°C by pressing the  
key. (200°C need be set for NO/CO analyzer.)  
or  
key and determine it by the ENT  
(c) Parameter need not be set because they have been factory-set.  
(d) The temperature controller controls converter temperature through the SSR relay.  
(8) Setting of pressure control valve  
The pressure control valve has been set the discharge about 2 N/min. of sample gas together with drain,  
when the pressure at the inlet is about 50 kPa. The set pressure increases with a right turn of the setting knob  
and decreases with a left turn.  
Do not turn the setting knob unless the sample flow needs to be changed.  
Setting knob  
2-Rc1/4  
Sample  
OUT  
IN  
Fig. 10-7 External appearance of pressure control valve  
33 –  
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(9) Washing the Permapure dryer  
The Permapure dryer is used for SO2 measurement (2000 ppm or more).  
The Permapure dryer has no moving sections nor consumable parts. If precautions in using it are suffi-  
ciently respected, it can operate without maintenance usually. However, if its element has clogged, for  
example, remedy it by the following method.  
Purge IN  
Header  
Element tube  
Purge joint  
Shell joint  
Sample  
OUT  
Sample  
IN  
Shell  
Sample joint  
O ring presser  
Tee  
Purge OUT  
O ring  
Fig. 10-8 Structure of Permapure dryer  
(a) Disassembly  
q Remove an O ring presser (one side).  
w Loosen a shell joint (one side).  
e Push the header inward and remove the tee.  
r Loosen the other shell joint and gently pull out the element.  
(b) Washing  
q Carry out washing with tap water (detergent, alkali solution not allowed).  
w On a side, remove the sample joint, cap and tee.  
e Through the opposite port and purge port, introduce tap water at 127 kPa or lower pressure and  
300 to 500 mN/min of flow rate.  
r Carry out washing for longer or shorter time according to the degree of clogging.  
If the clogging is slight, approximately 1 hour of washing is enough.  
Tap water  
Tap water  
Element tube  
Permapure dryer  
Fig. 10-9 Washing of Permapure dryer  
34 –  
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10.6 Maintenance of zirconia O2 sensor  
Sensor temperature  
OXYGEN ANALYZER  
800  
POWER  
ON  
1
2
3
4
5
6
7
OFF  
+
AG  
0V  
ALM  
Power SW Fuse 3A Terminal  
Front view  
Sample inlet Outlet (Rc 1/4)  
(Rc 1/4)  
Side view  
(1) Appearance of zirconia O2 sensor  
(2) Routine maintenance  
No parts require periodic maintenance. In case sensor temperature is 800±5°C or the SO2 concentration in  
sample gas is high, you should check occasionally that the outlet pipe is not clogged by the precipitation of  
crystal. Because the sample outlet is at a high temperature, attention should be paid not to suffer a burn.  
10.7 Others, major component figures  
Rc1/4  
Gas outlet  
Up  
2-Ø4.5  
mounting holes  
19  
Mounting direction  
Ø20 panel cutout  
Gas intlet  
Rc1/4  
34  
5
31  
Approx. 25 (when fully open)  
35 –  
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11. STANDARD ACCESSORIES AND SPARES  
Caution  
Do not use replacement parts which are not specified by makers. Use of these parts will not only  
provide the required performance but also result in damage or other trouble.  
Replacement parts used for maintenance must be handled as incombustible objects.  
11.1 Standard accessories  
Quantity (analyzer)  
No.  
Part name  
Type of part No.  
Remarks  
NOX/SO2 NOX  
SO2  
2
Other  
1
2
Membrane filter paper  
TK701837C6  
TK741833P3  
1 pack  
1 pack 25 sheets per pack  
Flouro pour filter for  
membrane filter  
2
3
4
5
Fuse (for instrument switch) Various types  
2 each 2 each 2 each 2 each For 2A, 3.2A  
Cooler puller  
Joint  
1
1
1
1
TK7F7627P1  
1 set  
1 set  
1 set  
1 set  
Measuring number of gases + 1  
For pressure regulator  
6
Hose band  
TK539474C410  
100% 100% 100% 100%  
For ø6 tube  
For pressure regulator  
7
8
9
Toalon tube 0.3m  
Polyethylene tube 1m  
Anchor bolt  
TK727528P1  
415966P4  
1
1 set  
4
1
1 set  
4
1
1 set  
4
1
1 set  
4
For ø6 tube  
ø6/ø4 For standard gas  
Option  
M12 x 160 x 50  
10 Instruction manual  
INZ-TN2ZSP  
INZ-TN2ZRG  
1
1
1
1
11 Analyzer accessories  
1 set  
1
1 set  
1
1 set  
1
1 set  
1
Infrared analyzer fuse 2A x 2pcs.  
Cell cleaning cloth x 1pc.  
O2 analyzer fuse x 1pc.  
12 Wash bottle  
TK7H3493P1  
For conditioner  
Note) Part No. 8 will be shipped in connection with the solenoid valve in the locker.  
36 –  
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11.2 Spares for 1 year (optional)  
Quantity (analyzer)  
No.  
Part name  
Spare for converter  
Remarks  
TK726889C3  
NOX/SO2 NOX  
SO2  
2
Other  
1
2
3
4
5
6
7
8
Note 2)1  
1
2
2
Catalyst and filter  
TK7H8043P1  
Conditioner filter  
2
2
Conditioner O-ring  
2
2
2
G65 chloproprene 8553765  
25 sheets of TK701837C6 per pack  
TK741833P3  
Membrane filter paper  
Fluro pour filter for membrane filter  
Membrane filter rubber ring  
Membrane filter O-ring  
Capillary  
6
1
pack  
1
6
1
pack  
1
1
1
Chloroprene  
G65 chloroprene  
For 0.5 K  
TK733572P1  
8553765  
1
1
1
1
1
1
(only when with pressure control valve)  
9
Capillary (for bypass)  
1
1
1
1
1
1
1
1
TK729264C6 (ø1mm)  
(only when without pressure control valve)  
10 Capillary (for cooler out)  
TK729264C7 (ø1.4mm)  
(only when without pressure control valve)  
11 Aspirator diaphragm  
12 Aspirator valve  
1
1
1
2
1
1
1
2
1
1
1
2
1
1
1
2
TK725417P5  
TK725417P6  
When gas extractor is  
simultaneously supplied.  
(ZBAK1)  
13 Gas extractor filter element  
TK7H8439P1  
85504N3  
14 Gas extractor O-ring  
P48A  
Note 1) The contents of standard accessories, and spares and supplies for 1 year may vary somewhat  
according to the specifications.  
Note 2) Two parts are required when flow rate is 0.5N and NO range is beyond 200 ppm.  
Code for preparation of 1-year spares and supplies  
Analysis gas  
NOx, SO2, (CO), (O2)  
Same as above  
NOx, (CO), (O2)  
Same as above  
SO2, (O2)  
Extractor  
With  
Code  
Remarks  
ZBN4SP12  
ZBN4SP22  
ZBN4SP32  
ZBN4SP42  
ZBN4SP52  
ZBN4SP62  
ZBN4SP72  
ZBN4SP82  
SO2 meter range 200 to 1000ppm  
SO2 meter range 200 to 1000ppm  
Without  
With  
Without  
With  
SO2 meter range 200 to 1000ppm  
SO2 meter range 200 to 1000ppm  
Same as above  
CO, (O2)  
Without  
With  
Same as above  
Without  
37 –  
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12. PROCESSING OF HEATING PIPE ENDS  
12.1 Outline  
(1) Configuration  
Power supply 100VAC, 50/60Hz  
Power connection kit  
About 2000  
Heating pipe  
Termination kit  
About 500  
Fig. 12-1  
(2) Caution on connection of heating pipe  
q
The clearance between clamp supports must be about 1.2 m in the horizontal direction and about 3 m in  
the vertical direction.  
w
For a bent piping, bending should be moderate enough to ensure a minimum bending radius of 300 mm  
or more.  
Clamp support  
No good  
Good  
Fig. 12-2  
(3) Connection diagram  
A heater wire is wound around 2 isolated buses and it is brought into contact with the buses alternately at  
intervals of 300 mm (heating unit).  
Power supply  
Heating wire  
300mm  
300mm  
300mm  
300mm  
300mm  
300mm  
Fig. 12-3  
38 –  
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12.2 End processing method  
(1) Power supply side (power connection kit)  
q
w
When cutting out the heating pipe, take care not to damage the heater wire.  
Pulling out on the inside of grid section provides a non-heating area of about 300 mm at maximum.  
Grid  
Non-heating area of 300mm long  
Fig. 12-4  
e
Peel the outer sheath covering of heater as shown below and cut off the heater wire as close to its root  
as possible.  
(HTP type heater has fiber glass, heater wire and thin Teflon covering under its outer sheath covering.  
So the outer sheath covering should be peeled neatly.)  
115 mm  
Cut off at root.  
Fig. 12-5  
r
Apply RTV (silicone sealant) to the terminal boots and plug the boots into the heater. Then wind a  
sealing tape across the boots and heater.  
RTV  
RTV  
Terminal boots  
10  
Fig. 12-6  
t
For connection with the power supply wire, use a press-fitting sleeve. If the press-fitting section is  
loose, contact resistance becomes large to cause abnormal heating of the sleeve.  
Fig. 12-7  
39 –  
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(2) Termination side (termination kit)  
q
Cut the heater in the dimension shown at right.  
Grid  
Grid  
Push back the metallic braiding and fix it with  
Teflon tape.  
40mm  
300mm  
w
Peel the outer sheath covering of heater and cut  
off the heater wire as close to the root as pos-  
sible. Expose the bus of heater wire toward the  
cut end starting from a point about 40 mm away  
from the nearest grid. (HTP type heater has fi-  
ber glass, heater wire and thin Teflon covering  
under its outer sheath convering. So the outer  
sheath covering should be peeled neatly.)  
150 mm  
Grid area  
Outer sheath  
covering  
Metallic  
braiding  
Teflon tape  
Inner sheath covering  
Outer sheath covering  
12mm  
e
r
Cut off buses at different lengths.  
Bus  
Cut off at root  
Heater wire  
Wind Teflon tape while carefully securing isola-  
tion between the heater wire and buses.  
6mm  
Outer sheath covering  
Inner sheath covering  
Teflon tape  
t
Apply RTV silicone sealant to the end cap and  
the Teflon tape-wound section. Then, fit the end  
cap while bleeding air.  
RTV silicone sealant  
Note) After fitting the cap, move it back  
slightly.  
Fit while turning  
End cap  
Seal tape  
y
Fix the end cap by winding seal tape as many  
times as possible for preventing the cap from slip-  
ping off.  
Note) Never short-circuit the end (bus) of  
heater.  
40 –  
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12.3 Check after piping  
q
w
e
r
t
y
The heating pipe is not sunk significantly due to a clamp, etc.  
The bent section has an adequately large bending radius.  
Electrical connections are exact.  
The end of heater wire (bus) is not short-circuited (it must never be short-circuited).  
All parts of the connection kit (sealing connector), etc. have been used.  
Screws of the connection kit (sealing connector), etc. have been tightened completely.  
12.4 Clamp support  
Clamps for conduit should be used. For heating pipe profile of the tube trace, refer to 12.5.  
The heating pipe should be clamped so that it will be sunk significantly.  
No good  
Good  
Fig. 12-8  
41 –  
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12.5 Specifications of tube trace  
(1) Structure of tube trace  
1
4
Heater cable  
PFA teflon  
3
2
5
q
w
e
r
t
Heater cable (power limiting cable)  
Process tube  
Aluminum tape  
Fiber glass heat insulator  
PVC jacket  
Fig. 12-9  
(2) Specifications of tube trace  
q
w
e
r
t
Heater cable  
Process tube  
Aluminum tape  
Fiber glass  
HPT 20-1 BN 35.4w/m at 100ºC (100V AC)  
10/8 mm øPFA Teflon tube  
50% overlap  
Thermal conductivity 0.2kJ/m·h·ºC  
UL 105ºC, black PVC  
PVC jacket  
12.6 Specifications of heating pipe  
Maker: Thermon Far East  
Dealer: Fujikin, Japan  
42 –  
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13. TROUBLESHOOTING  
Caution  
When trouble cannot be remedied even after following the instruction manual, contact your dealer or  
Fuji's service station (serivice engineer). Do not disassemble the device, as it results in electric shocks  
or injury.  
13.1 Troubleshooting of instrument  
Trouble  
Decrease of sample Filter (primary, second-  
gas flow rate ary, tertiary filters)  
Probable location  
Check item  
Remedy  
Check if filter element is clogged.  
Clean or replace element.  
Diaphragm type aspirator Check if aspirator is working normally.  
Check for abnormal sound or vibration.  
Clean or replace.  
Retighten screws or replace  
aspirator.  
Electronic gas cooler  
Check if cooler is working normally,  
check cooling temperature and check for  
clogging of flow path.  
Clean or replace.  
Conditioner  
Gas leakage  
Flowmeter  
Water decreases in lower chamber.  
Inject water and check the  
capillary (bypass).  
Check for gas leakage in piping after  
aspirator or at joints.  
Retighten or replace parts.  
Check for accumulation of drainage or  
dust in flowmeter. Check adjustment of  
needle valve.  
Clean the flowmeter.  
Adjust needle valve.  
Piping, capillary  
Check for bent or clogged piping.  
Check for capillary.  
Replace.  
Increase of bubbling Bypass flow path  
Clean or replace.  
Connect properly.  
Disassemble and clean.  
flow rate  
Piping  
Check for deviated joint.  
Rise of sample gas  
Pressure control valve  
Pressure control valve is clogged.  
flow  
(Note)  
Indicated value is  
abnormal.  
Gas leakage  
Check for gas leakage in parts before  
aspirator such as secondary coarse filter  
holder, piping, joints, etc.  
Retighten or replace parts.  
Diaphragm  
type aspiration  
Check if aspirator is normally operating  
and sample gas is flowing at set value.  
Clean aspirator or replace  
parts such as diaphragm or  
value  
Adjust sample gas flow.  
Conditioner  
Check if water level is normal.  
Check if air is aspirated.  
Supply water.  
Check primary filter.  
Dissolution of gas  
Sampling pipe  
Check for accumulation of drainage in  
piping.  
Clean, and tilt piping so  
drainage does not accumulate.  
Check if SUS pipe is used (for SO2  
analyzer).  
Change to teflon tube.  
Note) Pressure control valve is used.  
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Trouble  
Probable location  
Gas leakage  
Check item  
Remedy  
Check for gas leakage before the  
aspirator.  
Retighten or replace parts.  
Indicated value is  
not as expected.  
Interference due to  
moisture  
With respect to zero gas indication, the  
indicated value when air is introduced  
exceeds ±2% full scale.  
Readjust to compensate for  
moisture interference.  
Measuring range  
Zero, span  
Check if correct range is set.  
Reset the range.  
Check zero and span using standard gas. Adjust for correct zero  
point and span.  
Cell window  
Check if cloudy  
Clean the window.  
Replace the fuse.  
Power supply, fuse  
Check the power supply voltage and fuse.  
Indication doesnt  
change  
13.2 Error codes and remedies  
This analyzer is provided with self-diagnosis functions, and an error code is displayed if an abnormality  
occurs in the instrument.  
Take a proper measure with reference to the instruction manual of infrared gas analyzer when an error code  
appears.  
44 –  
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14. SPECIFICATIONS  
Specifications  
Type of cubicle:  
Outdoor, self-standing, sealed type or indoor type  
Non-dispersion infrared absorption (NDIR method) for NOx, SO2, CO and CO2;  
zirconia method for O2.  
Measuring system:  
Sampling system:  
Measuring range:  
Dry sampling electronic cooling & dehumidification system  
(Permapure dryer adopted)  
NOx 0 to 100 .... 2000 ppm  
SO2 0 to 100 .... 1000 ppm  
(Range selection:  
Max. rate 1:20  
(except for O2))  
CO 0 to 200 .... 2000 ppm  
CO2 0 to 5 ........ 50%  
O2 0 to 10/25%  
Note: Measuring range of each gas is 50 to 5000ppm, available in  
approved type (special order).  
Repeatability:  
Drift:  
±0.5% of full scale  
Zero ±2% of full scale/week for NOx, SO2 and CO  
±2% of full scale/month for O2  
Span ±2% of full scale/week  
Linearity:  
±2% of full scale  
Response time:  
90% response from the inlet of cubicle  
SO2 : 4 min. CO : 2.5 min NO : 2 min  
Others : 3 min.  
Output:  
4 to 20mA DC (allowable load resistance 550), non-isolated.  
For the number of output points, see Table 1.  
Contact output:  
Indication:  
Each NO (1a) contact (100V AC, 1A) for error (analyzer error, calibration error) and  
auto calibration status  
Digital indication (indicating measured value and measuring range on analyzer front  
panel of infrared gas analyzer)  
Sample gas extracting rate: Approx. 2 N/min.  
Gas extractor:  
Electrical heating type (filter built in)  
Filter mesh 40µm mesh of 316 stainless steel  
Probe  
316 stainless steel, length 600, 800 or 1000mm  
JIS 5 K65AFF  
Flange  
Sample inlet tube:  
ø 10/ ø 8mm teflon tube for CO and O2 meter and NOx and O2 meter  
Heating tube ( ø 10/ ø 8mm teflon tube) for NOx, SO2 and O2 meter and NOx, SO2, CO  
and O2 meter  
Standard gas (3.4 N):  
Standard air gas for zero calibration and O2 span calibration  
Standard analyte/remaining N2 gas for low range span calibration and O2 zero calibration  
Form for all components already approved  
Form verification:  
Ambient temperature:  
Power supply:  
-5 to +40°C  
100±10V AC, 50 or 60Hz  
Power consumption:  
Mass (weight):  
Approx. 1,200 VA (excluding consent and heating tube)  
Approx. 300 kg (excluding standard gas)  
Finish color:  
Munsell 5Y 7/1 semigloss  
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Standard requirements  
for sample gas:  
Temperature —  
60 to 800°C  
100 mg/Nm3 or less  
2.94 to +2.94kPa  
Dust  
Pressure  
-
Components SO2 0 to 1000ppm  
NOx 0 to 2000ppm (NO2 100ppm or less)  
CO2 several % to over 10%  
CO 0 to 2000ppm  
O2 0.5 to 21%  
H2O 0 to 40%  
HCN 0 to 100ppm  
N2 remaining percent  
When other components are contained in the sample gas, consult with Fuji.  
Note) NO2/NO converter catalyst life:  
1 year/NO2, 10ppm  
1 month/NO2, 100ppm  
Installation requirements:Select a location free from direct sunlight and severe vibration.  
Table 1 Number of output points and kinds of outputs  
Type  
ZSP1L  
ZSP1F  
ZSP1P  
ZSP1B  
CO, O2  
ZSP1A  
ZSP1H  
ZSP1M  
Measuring  
component  
NOx, SO2,  
CO, O2  
NOx, SO2,  
O2  
NOx, O2  
SO2, (O2)  
NOx, CO2, O2  
NOx, SO2,  
CO, CO2, O2  
No. of  
11  
7
3
3
3
5
12  
output points  
Kind of output A, B, C,  
A, B, D, E,  
A, D, E  
C, D, K  
B, (D)  
A, B, D, E, K  
A, B, C,  
D (2 points), E, F, H, J  
D (2 points),  
E, F, G, H, J,  
K, L  
F, G, H, J, K  
A: NOx instantaneous value  
C: CO instantaneous value  
B: SO2 instantaneous value  
D: O2 instantaneous value  
E: NOx instantaneous value after O2 correction  
G: CO instantaneous value after O2 correction  
J: 1hr. moving average SO2 value after O2 correction  
L: O2 instanteneous value  
F: SO2 instantaneous value after O2 correction  
H: 1hr. moving average NOx value after O2 correction  
K: 4hr. moving average CO value after O2 correction  
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(1) NOx after O2 correction  
CO after O2 correction  
(a) Calculating equation  
21 - On  
C=  
Cs  
21 - OS  
C: Concentration after O2 conversion  
Cs: NOX or CO concentration measured  
Os: O2 concentration measured  
On: O2 concentration as conversion basic:  
4% Oil combustion boiler  
5% Gas combustion boiler  
6% Solid object combustion boiler, petroleum heating furnace  
12% Garbage incinerator  
(b) Block diagram  
NOx or  
CO signal  
O
2/NOx conversion  
21 - On  
21 - Os  
· Cs  
or CO (ppm)  
Zurconia  
type O2 sensor  
O
2
O
2
converter  
signal  
Full scale is the same as  
instantaneous value before  
conversion.  
Infrared gas analyzer  
(2) Moving average output  
1 hr. moving average output (for NOx, SO2)  
4 hr. moving average output (for CO)  
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Automatic calibration  
Calibration tolerance:  
±0.2% FS  
Automatic calibration output hold: Possible  
(Example in 4 component analyzer):  
CO zero  
CO span  
O2  
zero  
NOx, SO2 zero  
NOx span  
SO2 span  
O2  
span  
Automatic  
calibration  
Calibration cycle:  
Calibration gas feed time:  
Display:  
Once/day (variable, up to 7 days)  
2 to 10 min. (variable), common to each gas  
Calibration failure  
Error code (E-) is displayed when one-time calibration volume is more  
than ± 20% FS on both zero and span and it is under calibration:  
CAL lamp ON  
Ordering information  
1. Measuring range of analyzer  
2. Length of sampling pipe  
3. Insertion length of sampling tube  
4. Power voltage/frequency  
5. Instruction required when standard gas is not necessary  
6. Instruction required when individual inspection is not necessary  
7. Necessity of spares and supplies (for 1 year)  
8. Additional functions  
Note: When special functions such as remote range selection, output hold by external contact, auto-  
matic calibration, automatic calibration start by external contact, insulation output, measured  
value concentration alarm, etc. are required, they should be separately designated.  
48 –  
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CODE SYMBOLS  
1
Z
2
S
3
P
4
5
6
7
8
4
9 10 11 12  
Descrption  
Application  
Combustion exhaust gas (standard condition)  
Other exhaust gas  
1
2
Component  
NOX + (O2  
)
P
A
B
F
CO + (O2  
)
SO2 + (O2  
)
NOX + SO2 + (O2  
)
NOX + SO2 + CO + (O2  
NOX + SO2 + CO + (O2  
Others  
)
)
H
L
Z
Oxygen analyzer  
Without  
With ZFK  
0
1
3
With ZKG (Non-standard)  
Auto calibration  
1
With  
Type of cubicle  
Indoor installation type  
Outdoor installation type  
1
2
External piping  
Heating pipe  
ø10 Teflon tube  
1
2
Standard gas  
3.4r  
10r  
3.4r + instrument air  
10r+ instrument air  
3.4r + atmopheric air  
10r+ atmopheric air  
1
2
3
4
5
6
Power supply  
100V AC/50Hz  
100V AC/60Hz  
Others 50Hz  
5
6
9
0
Others 60Hz  
49 –  
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SAMPLING SYSTEM BLOCK DIAGLAM  
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Functions of individual components  
Gas extractor (type; ZBA):  
With heating type stainless steel filter; standard diameter 40µm for filter.  
Gas conditioner (type; ZBH9)  
For separating drain and removing sulfuric acid mist and oil mist or fine dust particles. Besides, for  
preventing aspiration of drain at clogging of extractor filter or sampling pipe, and activating composite  
operation of constant-pressure bubbler for maintaining a constant sample supply to analyzer.  
Aspirator (type; ZBG8)  
For aspirating sample gas (sample gas flow rate: about 2N/min.)  
Electronic gas cooler (type; ZBC)  
An electronic dehumidifier which dries the moisture in sample gas to a dew point of aproximately 2°C.  
Converter (type; ZDL):  
Added to the NOx analyzer. A converter using a special catalyst which converts NO2 gas into NO. The  
catalyst must be renewed annually (built in the temperature regulator).  
Solenoid valve (type; AB21)  
Used for the introduction of calibration gas.  
Memberane filter (type; ZBBM)  
Eliminates fine dust particles with glass-fiber or flouropore filter, and permits monitoring dust adher-  
ing condition on the front of the body.  
Flow meter (type; ZBD)  
Ajusts and monitors standard flow rate of sample gas.  
Standard gas (type; ZBM):  
Reference gas used for calibrating zero and span of the analyzer. When using a zirconia oxygen meter,  
this is used together with air for calibrating zero for NO, SO2, and CO and for calibrating span for O2.  
Zirconia O2 sensor (type; ZFK3, 4)  
Used in combination with the infrared analyzer. Outputs about 0V at measurement of the air, and an  
inverse logarithm of about 1V at measurement of 0.05% O2.  
Pressure control valve (type; ZBD35)  
Sample gas pressure is controlled to 49kPa to maintain a constant flow rate.  
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OUTLINE DIAGRAM (Unit:mm)  
For outdoor installation type  
Anchor plan and door opening  
diagram  
1000  
815  
620  
Cable inlet (60 × 120  
Rear  
side  
rectangular hole)  
with plastic resin-  
cover (PVC)  
Rc 3/8  
Front  
side  
A-140-2-1  
(key No.200)  
Anchor bolt (option)  
( 4 M12 × 160 × 50 )  
Rc 1/2  
760  
800  
620  
800  
4-φ15 hole  
For indoor installation type  
Anchor plan and door opening  
diagram  
800  
800  
620  
Cable inlet (60 × 120  
Rear  
side  
rectangular hole)  
with plastic resin-  
cover (PVC)  
Rc 3/8  
Front  
side  
A-140-2-1  
(key No.200)  
Anchor bolt (option)  
( 4 M12 × 160 × 50 )  
850  
Rc 1/2  
760  
800  
620  
800  
4- φ15hole  
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CONNECTION DIAGRAM  
1
L1  
L2  
G
Power supply  
100V AC  
2
3
4
5
J1  
J2  
Extractor  
6
7
H1  
H2  
A1  
A2  
A3  
A4  
B1  
Heating tube  
8
9
NOx instantaneous value  
NOx average value  
SO2 instantaneous value  
10  
11  
12  
13  
14  
15  
16  
17  
18  
19  
20  
21  
22  
23  
24  
25  
26  
27  
28  
29  
30  
31  
32  
33  
34  
35  
36  
B2  
B3  
SO2 average value  
B4  
C1  
O2  
instantateous value  
C2  
C3  
NOX instantateous value  
SO2 corrected value  
C4  
C5  
C6  
C1A  
C2A  
E1  
O2  
instantateous value  
CO instantaneous value  
CO average value  
E2  
E3  
E4  
C7  
CO corrected value  
C8  
D11  
D12  
D21  
D22  
Failure contact output  
On maintenance and auto  
calibration contact output  
Note: Terminal numbers are fixed.  
(only specified outputs are wired).  
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Head Office  
Gate City Ohsaki, East Tower, 11-2, Osaki 1-chome,  
Shinagawa-ku, Tokyo 141-0032, Japan  
Instrumentation Div.  
International Sales Dept.  
No.1, Fuji-machi, Hino-city, Tokyo 191-8502, Japan  
Phone: 81-42-585-6201, 6202 Fax: 81-42-585-6187  
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