Hach Sander 3650 ATEX User Manual

Operator Quick Guide  
ORBISPHERE 3650 ATEX  
Revision D - 18/03/2008  
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Measurement  
Gas concentration measurements are displayed  
Taking Measurements  
for about two minutes. After two minutes the  
instrument displays the sample number (starting  
at 000), then the gas concentration measurement  
value followed by [---] to indicate the  
measurement is being stored.  
Connect the top-mounted inlet to accept your  
sample, typically this is accomplished by  
connection to a sampling valve. The sample flow  
can be regulated by the knurled stainless steel  
knob on top of the flow chamber.  
This storage sequence repeats automatically, at  
the rate specified.  
The LCD includes a right-side marker to  
distinguish between gas concentration  
measurements and temperature. To switch  
between gas measurement and temperature  
measurement, press the × Ø buttons. To  
backlight the LCD for approximately three  
minutes, press the Backlight button.  
To end automatic storage, switch the instrument  
OFF (by pressing the POWER key) while it is in  
normal measurement mode. Switching ON again  
without holding down the STO button returns the  
instrument to measurement mode.  
The analyzer will store up to 500 gas  
measurement values, labeled by numbers 0  
through 499, along with the current date and time  
of each measurement. You have the choice of  
acquiring this information manually or  
automatically, as described below.  
Manual Data Acquisition  
Automatic Data Acquisition  
Before starting automatic measurement storage,  
first select the sampling rate desired using the  
Sampling Rate menu of the WinLog97 program.  
For the first measurement you wish to store, press  
the STO button once to display a sample number.  
The default sample number is 000(for first time  
access), or the last used memory position where  
data was stored, incremented by a value of 1.  
You can increase or decrease this number by  
pressing the × Ø buttons within three seconds.  
Press STO a second time, within five seconds of  
the first. The instrument then displays the gas  
concentration measurement value for about three  
seconds, followed by a clearing message as the  
value is stored.  
Switch the instrument OFF (by pressing the  
POWER key). Then hold down the STO button  
while switching the instrument back ON. The LCD  
displays the message Stofor about one second.  
Repeat the above steps to store additional  
measurements.  
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Measurement (cont)  
DownLoad data command from the Logger  
menu.  
Viewing Stored Measurements  
The window displays the stored measurements  
from the instrument showing the sample number,  
gas concentration, a date and time stamp, and a  
sample description.  
Sample Description  
For help in identifying the locations of various  
sampling points that are stored by the analyzer,  
you may choose the Sampling Point  
Description command from the Logger menu.  
The measurement values to be placed in  
positions 0 through 499 can be described  
however you wish. Double-click on a particular  
position (or click Modify), then type a description  
in the box.  
Copy Data  
To copy the results to the Windows Clipboard, so  
that the data can be pasted into a spreadsheet,  
word processor or other Windows program that  
accepts tabular text information, choose the  
Clipboard command from the Export menu.  
Switch the instrument OFF (by pressing the  
POWER key). Hold down the × button while  
switching the instrument back ON. The LCD  
displays a sample location number.  
Save Data  
Scroll through the numbered sample locations of  
all the stored values using the × Ø buttons.  
To save this list of measurements as a text file,  
capable of being recalled by the WinLog97  
program or imported as a file into other Windows  
programs, choose the Save As command from  
the File menu and enter the device and file name.  
To view the actual gas concentration  
measurement value at a particular sample  
number, press the STO button. The LCD now  
displays the stored value for that sample number.  
Press STO a second time to return to the next  
numbered location display, to continue scrolling  
or view another stored value.  
Print Data  
To place this list of measurements into a tabular  
format and send it to the printer, choose the Print  
command from the File menu.  
To return to the measurement mode, switch the  
instrument OFF and then back ON again without  
holding down any additional buttons.  
Clear Data  
To clear all the values stored in the instrument,  
choose the Clear Data command from the  
Logger menu. Since this action will clear the  
storage memory of the instrument, a warning  
appears which you must confirm. Choose Clear  
to start the memory clear operation.  
Downloading Data  
If you have made measurements and stored them  
in the instrument, you should be ready to bring  
them into the WinLog97 program for viewing,  
copying, saving and printing. To download stored  
data from the instrument to the PC, choose the  
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Measurement (cont)  
Monitor Measurements in Real-Time  
You may wish to analyze a particular sampling point via the WinLog97 program's Monitoring menu. To  
use this Monitoring chart, the instrument must be connected to your PC.  
Choose Monitoring from  
the WinLog97 menu to  
bring up a chart display.  
The chart shows the gas  
concentration (in blue),  
temperature (in red), and  
pressure (in green) as the  
sample is being measured  
by the instrument. The  
chart is updated directly  
from  
instrument  
measurements, at a rate  
determined by the time  
scale  
set  
in  
the  
TIMEBASE box at the  
lower right corner of the  
chart.  
Click the TIMEBASE up/  
down pointers to change  
the time scale of the divisions of the chart. Each division mark along the baseline (1, 2, ...10) can be  
made to represent from 30 seconds to 2½ hours, providing from 5 minutes to 25 hours of continuously  
displayed samples (as illustrated in the table).  
Click on the Continuous box to enable or  
disable continuous charting. When this box is  
checked, the chart scrolls continuously after  
reaching the 10 division, and the oldest  
samples are lost off the left of the chart.  
Timebase  
Updating Rate  
Max.  
Samples  
30 Seconds/Division  
1 Minute/Division  
10 Minutes/Division  
30 Minutes/Division  
1 Hour/Division  
5 Secs/Sample  
5 Secs/Sample  
5 Secs/Sample  
9 Secs/Sample  
18 Secs/Sample  
45 Secs/Sample  
60  
120  
When Continuous is not checked, the chart  
stops displaying new results after reaching  
the 10 division, and all subsequent  
measurements are lost.  
1,200  
2,000  
2,000  
2,000  
Click the up/down pointers for each  
2.5 Hours/Division  
measurement  
variable  
(GAS,  
TEMPERATURE and PRESSURE) to  
change the scaling of that value on the chart. The display of each measurement variable may be turned  
on or off by choosing the appropriate On or Off switch.  
A running display of latest sample Gas, Temperature and Pressure is also shown in the bottom-right  
corner of the chart.  
Use the buttons at the bottom of the chart to control real-time monitoring. Choose Go to clear the chart  
and start real-time monitoring, Stop to stop monitoring and Copy to copy the data from the chart as text  
information to the Windows Clipboard. This information can be pasted from the clipboard into any  
Windows application, such as a spreadsheet or word processor.  
Choose Close to close the Monitoring window.  
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Instrument Configuration  
The following commands are all available from  
MEMBRANE SELECTION  
the Configuration menu in the WinLog97  
software installed on your PC.  
You may find it necessary to use a different type  
of membrane for different applications.  
The instrument must be connected to your PC in  
order to change its configuration.  
INSTRUMENT - PC CONNECTION  
The Serial port menu lets you choose one of four  
serial communication ports. Usually, COM1 is  
used to connect to a mouse, so try COM2 first.  
To re-configure the analyzer, choose Membrane  
to bring up the box which reveals the membrane  
models available.  
CALIBRATION MODE  
Use the Calibration mode command to select  
how the sensor is to be calibrated.  
SETTING SAMPLING INTERVALS  
The analyzer can perform as a standalone data  
acquisition device, automatically recording gas  
measurements with the date and time, and storing  
up to 500 of these values.  
Choose In Air to allow calibration of the sensor in  
air, In Line to calibrate the sensor directly in the  
sampling line, or In a Span Gas to calibrate in a  
source of gas of known concentration.  
CALIBRATION KEY STATUS  
You can use the Calibration Key Status menu to  
prevent an accidental sensor re-calibration from  
the instrument keyboard.  
Choosing Sampling Rate lets you select time  
intervals (acquisition rate) for this storage  
capability.  
Enable or Disable the instrument front panel  
CAL button. Disabling the button will prevent  
accidental sensor re-calibration.  
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Instrument Configuration (cont)  
CALIBRATION RANGE CHECKING  
SPAN GAS  
When calibration is performed for In Air and In a  
Span Gas calibration modes, the sensor  
measurement current is compared to an ideal  
current for the selected membrane to determine  
whether or not to complete the calibration. You  
can use the Calibration Range Checking menu  
to enable or disable sensor calibration range  
checking in the instrument.  
When calibrating the sensor in a span gas, use  
the Span Gas menu to enter the span gas  
concentration (as a %age) when using a span gas  
as a calibration medium.  
DUAL USE (MODEL 3650Ex/113 ONLY)  
Use the Dual Use menu to change the  
measurement phase (either dissolved or  
gaseous) for the model 3650Ex/113 dual-use  
analyzer.  
Choose Disabled to calibrate without checking  
the value of the measurement current, within a  
range of 0% to 999% of the ideal current. When  
set to Enabled, at calibration the measurement  
current should be between 25% and 175% of the  
ideal current; if the value is outside of these limits,  
the calibration fails and Erris displayed on the  
instrument LCD.  
Choose ppm (dissolved) to set the instrument for  
dissolved measurement in liquids, or %  
(gaseous) to set the instrument to gas phase  
measurement.  
INSTRUMENT CONFIGURATION REVIEW  
To review if the instrument is set up as expected, choose the Configuration view command.  
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Calibration  
BAROMETRIC PRESSURE SENSOR  
Use the × Ø buttons to change the mode to your  
choice and press the STO button to set the  
selected mode.  
The instrument internal barometric pressure  
sensor is calibrated at the factory, and normally  
requires no further attention. However, you may  
wish to calibrate it against your own  
instrumentation, or simply check the instrument  
for accuracy.  
In a Span Gas Calibration  
The span gas calibration procedure may be used  
if you have a source of gas with a known  
concentration of O2 (in% units). To perform this  
Select Troubleshooting, Pressure Calibration  
from the WinLog97 program, and enter the  
current atmospheric pressure, in mbars, in the  
calibration pressure entry box.  
type of calibration, the instrument must be set for  
calibration In a Span Gas. The Windows  
WinLog97 program must also be used in this  
procedure.  
GAS SENSOR  
Switch on the instrument, if  
necessary, and wait a minute or  
The sensor can be calibrated either in air or  
directly in line in a liquid sample. Additionally,  
oxygen sensors can be calibrated using a span  
gas.  
so  
for  
the  
displayed  
measurement to settle. Then  
expose the sensor to a span gas  
sample with a known oxygen  
concentration. Enter the  
percentage of oxygen in the  
span gas using the WinLog97  
program.  
To perform a calibration, you must first choose  
which method you wish to use. The mode of  
calibration may be selected using the WinLog97  
program. Alternatively, you can select the mode  
of calibration using the instrument front panel  
buttons.  
Press the CAL button.  
Remember, this button may  
have been locked out to prevent  
an accidental reset.  
A brief clearing [---]message  
appears. Press CAL again  
within a 3 second period. The  
percentage of the measured  
current to the ideal one is  
displayed.  
When the reading is stable, press CAL again.  
If the new calibration current is within 25% to  
175% of the ideal current, the instrument displays  
CAL and returns to the measurement mode.  
Calibration is now complete, the sensor is  
calibrated, and you can proceed with your  
measurements.  
Switch the instrument power OFF. Switch the  
instrument on by holding down the CAL button,  
and then pressing the POWER button at the same  
time. The instrument display will show either Air  
for in air calibration, LIfor in line calibration, or  
SPAfor span gas calibration  
If the new calibration current is not within this  
range, the instrument displays Errand returns to  
measurement mode. The system will not  
calibrate, and it is likely that a sensor service will  
be required.  
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Calibration (cont)  
In Line Calibration  
In Air Calibration (oxygen sensors only)  
The oxygen sensor can be accurately calibrated  
in air. To perform this type of calibration, the  
instrument must be set for calibration In air.  
The in line calibration procedure can be used to  
calibrate the sensor directly in line, against a  
liquid sample with a known dissolved oxygen  
concentration.  
You can perform this procedure with the sensor  
connected to the instrument, but without the flow  
chamber mounted.  
To perform this type of calibration, the instrument  
must be set for calibration In line. Switch on the  
instrument, if necessary, and wait a minute or so  
for the displayed measurement to settle.  
The membrane must be dry, and prior to  
calibrating it may be necessary to remove the  
screw-on protection cap and its optional grill to  
make sure that the components are not damp.  
Expose the sensor to a liquid sample with a  
known gas concentration.  
Switch on the instrument, if necessary, and wait a  
minute or so for the displayed measurement to  
settle.  
Press the CAL button. Remember, this button  
may have been locked out to prevent an  
accidental reset.  
A brief clearing [---]message appears. Press  
CAL again within a 3 second period. A  
measurement will flash on the LCD, showing the  
oxygen concentration of the calibration sample.  
The process is then exactly the same as for  
calibration in a span gas, detailed previously.  
Assuming you know the gas content to be a  
certain value, you can adjust the displayed value  
with the × Ø keys.  
When the reading is adjusted to the known  
concentration, press CAL again. The instrument  
displays CAL and returns to the measurement  
mode.  
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Troubleshooting  
You may wish to use the Troubleshooting menu  
Type a number in the Number box (you may also  
select one of three units positions for the LCD's  
rightmost indicator bar as well). Then choose  
Send. The number and indicator bar placement  
should appear on your instrument LCD.  
to make sure that the instrument is configured  
correctly for your application, and is in good  
working order.  
The instrument must be connected to your PC to  
perform these tests.  
CLOCK SETTINGS  
SERIAL LINK TEST  
Choose the Clock settings option to set the date  
and time in the instrument.  
Normally, the instrument will inform you of a  
disconnected RS-232 (serial) link when  
appropriate. However, you can confirm a good  
connection using the Serial Link Test option, and  
echoing a test message via the instrument.  
ANALOG VOLTAGES VIEW  
Enter text characters in the Text to be sent box,  
then click Send. If the serial link is operating  
correctly, the exact same text will be displayed  
back from the instrument in the Echo box.  
The Analog Voltage View option gives a real-  
time look at voltages used by the system to  
transmit information about sensor current,  
temperature and pressure. This is useful when  
trying to identify an instrument problem with an  
Orbisphere service representative either on-site  
or over the phone.  
KEYBOARD TEST  
The Keyboard Test option will reveal whether all  
the instrument buttons are functioning correctly.  
The voltage limits for normal operation are:  
Current channel: -1.5 V to +1.5 V  
Press any one of the instrument's buttons (except  
the on/off button) for a full second or more. The  
appropriate square on-screen should darken.  
Temperature channel: +10 mV to +4 V  
Pressure channel: -100 mV to +100 mV  
DISPLAY TEST  
MEASUREMENTS VIEW  
Choosing the Display Test option lets you  
perform a one-way communication between  
computer and instrument.  
The Measurements View option confirms, on  
your PC monitor, what your instrument should be  
displaying on the LCD for gas concentration and  
sample temperature.  
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